CYCLOPROPYL 2,6-DIMETHYLPHENYL KETONE

Base Information

• Chemical Name: CYCLOPROPYL 2,6-DIMETHYLPHENYL KETONE
• CAS No.: 870002-28-1
• Molecular Formula: C₁₂H₁₄O
• Molecular Weight: 174.243
• Mol file: 870002-28-1.mol

Synonyms:CYCLOPROPYL 2,6-DIMETHYLPHENYL KETONE;Methanone,cyclopropyl(2,6-dimethylphenyl);

Chemical Property of CYCLOPROPYL 2,6-DIMETHYLPHENYL KETONE

Chemical Property:

• Vapor Pressure: 0.00596mmHg at 25°C
• Boiling Point: 272.8oC at 760 mmHg
• Flash Point: 111.7oC
• PSA: 17.07000
• Density: 1.07g/cm3
• LogP: 2.89610

Purity/Quality:

97% ^*data from raw suppliers

Cyclopropyl2,6-dimethylphenylketone 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of CYCLOPROPYL 2,6-DIMETHYLPHENYL KETONE

There total 1 articles about CYCLOPROPYL 2,6-DIMETHYLPHENYL KETONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

vinyl magnesium bromide (1826-67-1) + trimethylsulfoxonium iodide (1774-47-6) + 2,6-dimethylbenzaldehyde (1123-56-4) → cyclopropyl(2,6-dimethylphenyl)methanone (870002-28-1)

Guidance literature:

vinyl magnesium bromide; 2,6-dimethylbenzaldehyde; In tetrahydrofuran; at 0 - 20 ℃; for 2h; Inert atmosphere;

With manganese(IV) oxide; In diethyl ether; at 20 ℃; for 12h;

trimethylsulfoxonium iodide; With potassium tert-butylate; In dimethyl sulfoxide; at 20 ℃; for 4h; Inert atmosphere;

DOI:10.1021/jacs.1c01356

upstream raw materials:

vinyl magnesium bromide

trimethylsulfoxonium iodide

2,6-dimethylbenzaldehyde

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