Pyridine, 2-[(3-methylphenyl)azo]-

Base Information

Chemical Name:Pyridine, 2-[(3-methylphenyl)azo]-
CAS No.:87014-42-4
Molecular Formula:C12H11N3
Molecular Weight:197.239
Hs Code.:
DSSTox Substance ID:DTXSID10476575
Nikkaji Number:J2.096.665C,J489.768D

Synonyms:87014-42-4;Pyridine, 2-[(3-methylphenyl)azo]-;2-(m-tolylazo)pyridine;DTXSID10476575

Suppliers and Price of Pyridine, 2-[(3-methylphenyl)azo]-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Pyridine, 2-[(3-methylphenyl)azo]-

Chemical Property:

XLogP3:3.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:197.095297364
Heavy Atom Count:15
Complexity:215

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=CC=C1)N=NC2=CC=CC=N2

Technology Process of Pyridine, 2-[(3-methylphenyl)azo]-

There total 2 articles about Pyridine, 2-[(3-methylphenyl)azo]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 131972-14-0
{Ag(2-(m-tolylazo)pyridine)2}ClO₄

: 81600-80-8
RuCl₂(2-(m-tolylazo)pyridine)2

: sodium perchlorate

: 87014-42-4
2-(3-methylphenylazo)pyridine

: 139242-61-8
{Ru(2-(m-tolylazo)pyridine)3}(ClO₄)2*H₂O

Guidance literature:: In methanol; byproducts: AgCl; heated to reflux for 15 min; cooled, filtered, concd., addn. of an aq. soln. of NaClO4, pptn. filtered off, washed with diethyl ether, recrystn. (water or water-methanol 9:1); elem. anal.;

Reference yield: 70.0%

: 14898-67-0
ruthenium(III) chloride trihydrate

: 131972-14-0
{Ag(2-(m-tolylazo)pyridine)2}ClO₄

: sodium perchlorate

: 87014-42-4
2-(3-methylphenylazo)pyridine

: 139242-61-8
{Ru(2-(m-tolylazo)pyridine)3}(ClO₄)2*H₂O

Guidance literature:: In methanol; byproducts: AgCl; heated to reflux for 30 min; cooled, filtered, concd., addn. of an aq. soln. of NaClO4, pptn. filtered off, washed with diethyl ether, recrystn. (water or water-methanol 9:1); elem. anal.;

Reference yield: 95.0%

: 87014-42-4
2-(3-methylphenylazo)pyridine

: silver nitrate

: 131972-14-0
bis{2-(m-tolylazo)pyridine}silver(I) perchlorate

Guidance literature:: In methanol; soln. of Agno3 heated to reflux, addn. of soln. of ligand,mixt. heated to reflux for 3h, cooled; filtered, addn. of aq. NaClO4 with stirring, pptn., collected, washed (water), recrystd. (MeOH/water), dried (vac., P2O5); elem. anal.;
DOI:10.1016/S0277-5387(00)86950-8