2-ACETAMIDO-6-NITROBENZOIC ACID

Base Information

• Chemical Name: 2-ACETAMIDO-6-NITROBENZOIC ACID
• CAS No.: 73721-78-5
• Molecular Formula: C9H8N2O5
• Molecular Weight: 224.173
• Hs Code.: 2924299090
• Mol file: 73721-78-5.mol

Synonyms:Anthranilicacid, N-acetyl-6-nitro- (7CI);2-(acetylamino)-6-nitrobenzoic acid;2-acetamido-6-nitrobenzoic acid;Benzoic acid, 2-(acetylamino)-6-nitro-;

Chemical Property of 2-ACETAMIDO-6-NITROBENZOIC ACID

Chemical Property:

• Vapor Pressure: 1.01E-09mmHg at 25°C
• Melting Point: 214 °C(dec.)
• Refractive Index: 1.656
• Boiling Point: 472.2 °C at 760 mmHg
• Flash Point: 239.4 °C
• PSA: 112.22000
• Density: 1.526 g/cm³
• LogP: 1.84760
• Storage Temp.: Inert atmosphere,Room Temperature
• Solubility.: soluble in Methanol

Purity/Quality:

97% ^*data from raw suppliers

2-(Acetylamino)-6-nitrobenzoicAcid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-ACETAMIDO-6-NITROBENZOIC ACID

There total 6 articles about 2-ACETAMIDO-6-NITROBENZOIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.5%

2-methyl-5-nitro-4H-benzo[d][1,3]oxazin-4-one (412341-84-5) → 2-acetamido-6-nitrobenzoic acid (73721-78-5)

Guidance literature:

With water; for 0.5h; Reflux;

Reference yield:

6-nitroanthranilic acid (50573-74-5) + acetyl chloride (75-36-5) → 2-acetamido-6-nitrobenzoic acid (73721-78-5)

Guidance literature:

Alkaline conditions;

Reference yield:

2-methyl-5-nitro-4H-benzo[d][1,3]oxazin-4-one (412341-84-5) + acetic acid (64-19-7,77671-22-8) → 2-acetamido-6-nitrobenzoic acid (73721-78-5)

Guidance literature:

for 2191.5h;

upstream raw materials:

2-methyl-5-nitro-4H-benzo[d][1,3]oxazin-4-one

water

6-nitroanthranilic acid

acetyl chloride

Downstream raw materials:

6-acetylamino-anthranilic acid

rac-2-acetamido-N-(2,6-dioxopiperidin-3-yl)-6-nitrobenzamide

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