Carbamimidothioic acid, N-(2,3-dihydro-1,4-benzodioxin-6-yl)-N-methyl-, methyl ester

Base Information

Chemical Name:Carbamimidothioic acid, N-(2,3-dihydro-1,4-benzodioxin-6-yl)-N-methyl-, methyl ester
CAS No.:871214-52-7
Molecular Formula:C11H14N2O2S
Molecular Weight:238.31
Hs Code.:
Mol file:871214-52-7.mol

Synonyms:Carbamimidothioic acid, N-(2,3-dihydro-1,4-benzodioxin-6-yl)-N-methyl-, methyl ester

Suppliers and Price of Carbamimidothioic acid, N-(2,3-dihydro-1,4-benzodioxin-6-yl)-N-methyl-, methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Carbamimidothioic acid, N-(2,3-dihydro-1,4-benzodioxin-6-yl)-N-methyl-, methyl ester

Chemical Property:

PSA：68.15000
LogP:2.41860

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Carbamimidothioic acid, N-(2,3-dihydro-1,4-benzodioxin-6-yl)-N-methyl-, methyl ester

There total 2 articles about Carbamimidothioic acid, N-(2,3-dihydro-1,4-benzodioxin-6-yl)-N-methyl-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 77991-99-2
1-(2,3-dihydrobenzo[1,4]dioxin-6-yl)-3-methylthiourea

: 74-88-4
methyl iodide

: 871214-52-7
1-(2,3-dihydrobenzo[1,4]dioxin-6-yl)-2,3-dimethylisothiourea

Guidance literature:: In acetone; at 65 ℃; for 16h;
DOI:10.1016/j.bmcl.2005.08.056

Reference yield:

: 141492-50-4
6-isothiocyanato-2,3-dihydrobenzo[b][1,4]dioxine

: 871214-52-7
1-(2,3-dihydrobenzo[1,4]dioxin-6-yl)-2,3-dimethylisothiourea

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / ethanol / 3 h / 25 °C

2: 92 percent / acetone / 16 h / 65 °C

In ethanol; acetone;
DOI:10.1016/j.bmcl.2005.08.056