2-Oxa-4,7,10-triazaundecan-11-oic acid, 3-oxo-5-[[4-[2-oxo-2-(phenylmethoxy)ethoxy]phenyl]methyl]-1-phenyl-7-[ 2-[[(phenylmethoxy)carbonyl]amino]ethyl]-, phenylmethyl ester

Base Information

• Chemical Name: 2-Oxa-4,7,10-triazaundecan-11-oic acid, 3-oxo-5-[[4-[2-oxo-2-(phenylmethoxy)ethoxy]phenyl]methyl]-1-phenyl-7-[ 2-[[(phenylmethoxy)carbonyl]amino]ethyl]-, phenylmethyl ester
• CAS No.: 872462-22-1
• Molecular Formula: C46H50N4O9
• Molecular Weight: 802.924

Synonyms:

Chemical Property of 2-Oxa-4,7,10-triazaundecan-11-oic acid, 3-oxo-5-[[4-[2-oxo-2-(phenylmethoxy)ethoxy]phenyl]methyl]-1-phenyl-7-[ 2-[[(phenylmethoxy)carbonyl]amino]ethyl]-, phenylmethyl ester

Chemical Property:

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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Oxa-4,7,10-triazaundecan-11-oic acid, 3-oxo-5-[[4-[2-oxo-2-(phenylmethoxy)ethoxy]phenyl]methyl]-1-phenyl-7-[ 2-[[(phenylmethoxy)carbonyl]amino]ethyl]-, phenylmethyl ester

There total 2 articles about 2-Oxa-4,7,10-triazaundecan-11-oic acid, 3-oxo-5-[[4-[2-oxo-2-(phenylmethoxy)ethoxy]phenyl]methyl]-1-phenyl-7-[ 2-[[(phenylmethoxy)carbonyl]amino]ethyl]-, phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

(4-(2-benzyloxycarbonylamino-3-hydroxypropyl)-phenoxy)-acetic acid benzyl ester (872462-21-0) + N,N''-di-Z-diethylenetriamine (160256-75-7) → (4-(2-benzyloxycarbonylamino-3-(bis-(2-benzyloxycarbonylaminoethyl)-amino)-propyl)-phenoxy)-acetic acid benzyl ester (872462-22-1)

Guidance literature:

(4-(2-benzyloxycarbonylamino-3-hydroxypropyl)-phenoxy)-acetic acid benzyl ester; With 2,6-dimethylpyridine; trifluoromethylsulfonic anhydride; In dichloromethane; at -78 - 0 ℃; for 3.5h;

N,N''-di-Z-diethylenetriamine; With N-ethyl-N,N-diisopropylamine; In dichloromethane; at -20 - 20 ℃; for 30h;

Reference yield: 42.0%

C27H26F3NO8S + N,N''-di-Z-diethylenetriamine (160256-75-7) → (4-(2-benzyloxycarbonylamino-3-(bis-(2-benzyloxycarbonylaminoethyl)-amino)-propyl)-phenoxy)-acetic acid benzyl ester (872462-22-1)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at -20 - 20 ℃; for 30h;

Reference yield: 100.0%

(4-(2-benzyloxycarbonylamino-3-(bis-(2-benzyloxycarbonylaminoethyl)-amino)-propyl)-phenoxy)-acetic acid benzyl ester (872462-22-1) → (4-(2-amino-3-(bis-(2-aminoethyl)-amino)-propyl)-phenoxy)-acetic acid (872462-23-2)

Guidance literature:

With hydrogen; palladium 10% on activated carbon; In water; isopropyl alcohol; at 50 ℃; for 8h;

upstream raw materials:

N,N''-di-Z-diethylenetriamine

(4-(2-benzyloxycarbonylamino-3-hydroxypropyl)-phenoxy)-acetic acid benzyl ester

Downstream raw materials:

(4-(2-amino-3-(bis-(2-aminoethyl)-amino)-propyl)-phenoxy)-acetic acid

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