Technology Process of 9H-Carbazol-3-amine, 9-(4-methylphenyl)-
There total 3 articles about 9H-Carbazol-3-amine, 9-(4-methylphenyl)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrazine hydrate;
In
tetrahydrofuran; methanol; ethanol;
at 60 ℃;
for 1.08333h;
DOI:10.1016/j.tet.2013.07.040
- Guidance literature:
-
Multi-step reaction with 3 steps
1: copper nitrate hemi(pentahydrate); acetic acid; acetic anhydride / 0.75 h / 60 °C
2: potassium carbonate / 8 h / 180 °C
3: hydrazine hydrate; palladium 10% on activated carbon / tetrahydrofuran; ethanol; methanol / 1.08 h / 60 °C
With
copper nitrate hemi(pentahydrate); palladium 10% on activated carbon; acetic anhydride; potassium carbonate; hydrazine hydrate; acetic acid;
In
tetrahydrofuran; methanol; ethanol;
DOI:10.1016/j.tet.2013.07.040
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate / 8 h / 180 °C
2: hydrazine hydrate; palladium 10% on activated carbon / tetrahydrofuran; ethanol; methanol / 1.08 h / 60 °C
With
palladium 10% on activated carbon; potassium carbonate; hydrazine hydrate;
In
tetrahydrofuran; methanol; ethanol;
DOI:10.1016/j.tet.2013.07.040
