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Benzoic acid, 4-methoxy-, (2E)-2,5-hexadienyl ester

Base Information
  • Chemical Name:Benzoic acid, 4-methoxy-, (2E)-2,5-hexadienyl ester
  • CAS No.:872832-01-4
  • Molecular Formula:C14H16O3
  • Molecular Weight:232.279
  • Hs Code.:
Benzoic acid, 4-methoxy-, (2E)-2,5-hexadienyl ester

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Chemical Property of Benzoic acid, 4-methoxy-, (2E)-2,5-hexadienyl ester
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Technology Process of Benzoic acid, 4-methoxy-, (2E)-2,5-hexadienyl ester

There total 1 articles about Benzoic acid, 4-methoxy-, (2E)-2,5-hexadienyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/jo0518093
Guidance literature:
With potassium osmate(VI); methanesulfonamide; 1,4-bis(9-O-dihydroquinidine)phthalazine; In water; tert-butyl alcohol; at 0 ℃; for 2.25h;
DOI:10.1021/jo0518093
Guidance literature:
Multi-step reaction with 2 steps
1: 72 percent / AD-mix β; K2OsO4*2H2O; CH3SO2NH2 / 2-methyl-propan-2-ol; H2O / 2.25 h / 0 °C
2: p-toluenesulfonic acid / 1 h / 25 °C
With potassium osmate(VI); methanesulfonamide; toluene-4-sulfonic acid; 1,4-bis(9-O-dihydroquinidine)phthalazine; In water; tert-butyl alcohol;
DOI:10.1002/anie.200500556
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