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4-Methoxybenzoyl chloride suppliers in China
Cas No: 100-07-2
USD $ 3.0-3.0 / Kilogram 1 Kilogram 1-100 Metric Ton/Month Dayang Chem (Hangzhou) Co.,Ltd. Contact Supplier
Factory Supply Anisoyl chloride
Cas No: 100-07-2
No Data 1 1 Ality Chemical Corporation Contact Supplier
4-Methoxybenzoyl chloride suppliers in China CAS 100-07-2 P-Anisoyl Chloride Supplier in China
Cas No: 100-07-2
USD $ 1.0-2.0 / Kilogram 1 Kilogram 5000 Kilogram/Month Wuhan Monad Medicine Tech Co.,LTD Contact Supplier
High quality P-Anisoyl Chloride supplier in China CAS NO.100-07-2
Cas No: 100-07-2
No Data 1 Kilogram 500 Metric Ton/Month Shanghai PengMo Biotechnology Co.,Ltd Contact Supplier
High quality P-Anisoyl Chloride supplier in China
Cas No: 100-07-2
No Data No Data Metric Ton/Day Simagchem Corporation Contact Supplier
p-Anisoyl chloride
Cas No: 100-07-2
No Data No Data No Data Chemwill Asia Co., Ltd. Contact Supplier
p-Anisoyl chloride
Cas No: 100-07-2
USD $ 2.0-3.0 / Kilogram 1 Kilogram 50 Metric Ton/Day EAST CHEMSOURCES LIMITED Contact Supplier
Amadis Chemical offer CAS#100-07-2;CAT#A16143
Cas No: 100-07-2
No Data 10 Milligram Amadis Chemical Co., Ltd. Contact Supplier
4-Methoxybenzoyl chloride-
Cas No: 100-07-2
No Data 1 Kilogram 10000 Metric Ton/Year Henan Tianfu Chemical Co., Ltd. Contact Supplier
Factory supply p-Anisoyl chloride/4-Methoxybenzoyl chloride cas100-07-2
Cas No: 100-07-2
No Data 100 Gram 20000 Kilogram/Day Hubei XinRunde Chemical Co., Ltd Contact Supplier

100-07-2 Usage

Hazard

Solutions corrosive to tissue. Explosion risk when in closed containers due to pressure caused by decomposition at room temperature.

Chemical Reactivity

Reactivity with Water Reacts slowly to generate hydrogen chloride (hydrochloric acid). The reaction is not hazardous; Reactivity with Common Materials: Corrodes metal slowly; Stability During Transport: Stable; Neutralizing Agents for Acids and Caustics: Flush with water, rinse with sodium bicarbonate or lime solution; Polymerization: Not pertinent; Inhibitor of Polymerization: Not pertinent.

Safety Profile

Corrosive to skin, eyes, mucous membranes, and other tissue.Evolves HCl by hydrolysis. A storage hazard; can explode spontaneously at room temperature. When heated to decomposition it emits toxic fumes of Cland may explode.

Fire Hazard

Special Hazards of Combustion Products: Irritating hydrogen chloride fumes may be formed.

Uses

4-Methoxybenzoyl Chloride is used in the synthesis of stilbene and dihydrostilbene derivatives as potential anti-cancer agents. It is also used in the synthesis of coumarin dimers with potential HIV-1 activity.

Chemical Properties

colourless liquid

Health Hazard

Vapor irritates mucous membranes. Contact of liquid with eyes or skin causes severe irritation. Ingestion causes severe irritation of mouth and stomach.

General Description

An amber-colored crystalline solid. Melting point 72°F. Corrosive to metals and skin. Vapors may cause serious burns to the eyes.

Air & Water Reactions

Fumes in air. Reacts exothermically with water (including moisture in air or soil) to form hydrochloric acid and insoluble anisic acid [Merck 11th ed. 1989].

Reactivity Profile

ANISOYL CHLORIDE reacts exothermically with bases, including amines. Incompatible with water, strong oxidizing agents, alcohols. Sealed containers held at room temperature may explode, due to slow decomposition that builds up pressure. This situation is more dangerous with heat. May react vigorously or explosively with diisopropyl ether or other ethers in the presence of trace amounts of metal salts [J. Haz. Mat., 1981, 4, 291].

Uses

Intermediates of Liquid Crystals
InChI:InChI=1/C8H7ClO2/c1-11-7-4-2-6(3-5-7)8(9)10/h2-5H,1H3

100-07-2 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
TCI America (M0721)  4-Methoxybenzoyl Chloride  >99.0%(GC) 100-07-2 25g 180.00CNY Detail
TCI America (M0721)  4-Methoxybenzoyl Chloride  >99.0%(GC) 100-07-2 100g 540.00CNY Detail
TCI America (M0721)  4-Methoxybenzoyl Chloride  >99.0%(GC) 100-07-2 500g 1,680.00CNY Detail
Alfa Aesar (L13120)  4-Methoxybenzoyl chloride, 97%    100-07-2 25g 124.0CNY Detail
Alfa Aesar (L13120)  4-Methoxybenzoyl chloride, 97%    100-07-2 100g 318.0CNY Detail
Aldrich (A88476)  4-Methoxybenzoylchloride  99% 100-07-2 A88476-5G 145.08CNY Detail
Aldrich (A88476)  4-Methoxybenzoylchloride  99% 100-07-2 A88476-25G 298.35CNY Detail
Aldrich (A88476)  4-Methoxybenzoylchloride  99% 100-07-2 A88476-100G 711.36CNY Detail

100-07-2SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 10, 2017

Revision Date: Aug 10, 2017

1.Identification

1.1 GHS Product identifier

Product name 4-Methoxybenzoyl chloride

1.2 Other means of identification

Product number -
Other names p-Anisoyl Chloride

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:100-07-2 SDS

100-07-2Synthetic route

4-methoxybenzoic acid
100-09-4

4-methoxybenzoic acid

4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

Conditions
ConditionsYield
With thionyl chloride Reflux;100%
With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at 20℃; for 2h; Reflux;100%
With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at 35℃; for 1h;100%
p-methoxybenzotrichloride
3335-36-2

p-methoxybenzotrichloride

4-methoxybenzoic acid
100-09-4

4-methoxybenzoic acid

4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

Conditions
ConditionsYield
With iron(III) oxide at 128℃; for 2.3h; Autoclave;96.7%
carbon monoxide
201230-82-2

carbon monoxide

para-iodoanisole
696-62-8

para-iodoanisole

4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

Conditions
ConditionsYield
With bis(tri-t-butylphosphine)palladium(0); benzyltriphenylphosphonium chloride In toluene at 110℃; under 38002.6 Torr; for 24h; Glovebox; Autoclave; Inert atmosphere;95%
para-iodoanisole
696-62-8

para-iodoanisole

4-nitro-benzoyl chloride
122-04-3

4-nitro-benzoyl chloride

A

p-nitrobenzene iodide
636-98-6

p-nitrobenzene iodide

B

4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

Conditions
ConditionsYield
With (Xantphos)Pd(4-C6H4NO2)(I) In benzene at 90℃; for 20h; Kinetics; Solvent; Reagent/catalyst; Temperature; Sealed tube; Inert atmosphere;A n/a
B 95%
para-iodoanisole
696-62-8

para-iodoanisole

ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In toluene at 100℃; for 12h;89%
1-(4-methoxyphenyl)ethanone
100-06-1

1-(4-methoxyphenyl)ethanone

4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

Conditions
ConditionsYield
Stage #1: 1-(4-methoxyphenyl)ethanone With pyridine; disulfur dichloride In chlorobenzene at 20℃; for 2h;
Stage #2: With sulfuryl dichloride In chlorobenzene at 20 - 132℃; for 15.5h; Reagent/catalyst; Temperature;
86%
Stage #1: 1-(4-methoxyphenyl)ethanone With pyridine; sulfur monochloride In chlorobenzene at 20℃;
Stage #2: With thionyl chloride In chlorobenzene at 20 - 132℃;
63%
With pyridine; disulfur dichloride at 137℃; for 20h; Reagent/catalyst; Temperature; Concentration;91 %Spectr.
1-bromo-4-methoxy-benzene
104-92-7

1-bromo-4-methoxy-benzene

carbon monoxide
201230-82-2

carbon monoxide

4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

Conditions
ConditionsYield
With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; tri-tert-butyl phosphine; benzyltriphenylphosphonium chloride In toluene at 110℃; under 3040.2 Torr; for 24h; Kinetics; Catalytic behavior; Pressure; Reagent/catalyst; Solvent; Temperature; Inert atmosphere; Glovebox; Schlenk technique; Sealed tube;84%
t-butyl 4-methoxybenzoate
833-79-4

t-butyl 4-methoxybenzoate

4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

Conditions
ConditionsYield
With phosphorus trichloride In acetonitrile at 80℃; for 3h; Time; Schlenk technique;76%
With phosphorus trichloride In acetonitrile at 80℃; for 3h; Schlenk technique; Sealed tube;
para-iodoanisole
696-62-8

para-iodoanisole

aroyl chloride

aroyl chloride

4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In toluene at 100℃; for 12h;68%
(tris-tertbutylphosphine) p-anisoylpalladium chloride

(tris-tertbutylphosphine) p-anisoylpalladium chloride

4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

Conditions
ConditionsYield
With carbon monoxide In chloroform-d1 at 20℃; under 3800.26 Torr; for 0.166667h; Pressure; Temperature; Reagent/catalyst; Glovebox;59%
tetrachloromethane
56-23-5

tetrachloromethane

tert-butylhypochlorite
507-40-4

tert-butylhypochlorite

4-methoxy-benzaldehyde
123-11-5

4-methoxy-benzaldehyde

4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

1-(p-methoxybenzoyl)-3-methylimidazolium chloride
61166-15-2

1-(p-methoxybenzoyl)-3-methylimidazolium chloride

A

1-methyl-1H-imidazole
616-47-7

1-methyl-1H-imidazole

B

4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

Conditions
ConditionsYield
In dichloromethane at 25℃; Rate constant; Equilibrium constant;
4-methoxybenzoic acid
100-09-4

4-methoxybenzoic acid

A

benzoyl chloride
98-88-4

benzoyl chloride

B

4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

Conditions
ConditionsYield
With Benzotrichlorid; iron(III) chloride In benzene at 55℃; Product distribution; Rate constant; Thermodynamic data; ΔE(excit.), var. temp.;
1-(p-methoxybenzoyl)-3-methoxymethylimidazolium chloride
93342-84-8

1-(p-methoxybenzoyl)-3-methoxymethylimidazolium chloride

A

4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

B

1-(methoxymethyl)imidazole
20075-26-7

1-(methoxymethyl)imidazole

Conditions
ConditionsYield
In dichloromethane at 25℃; Rate constant; Equilibrium constant;
1-(p-methoxybenzoyl)-3-benzylimidazolium chloride
93342-85-9

1-(p-methoxybenzoyl)-3-benzylimidazolium chloride

A

1-benzylimidazole
4238-71-5

1-benzylimidazole

B

4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

Conditions
ConditionsYield
In dichloromethane at 25℃; Rate constant; Equilibrium constant;
4-methoxybenzoyl radical
2652-68-8

4-methoxybenzoyl radical

4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

Conditions
ConditionsYield
With tetrachloromethane In various solvent(s) at 22.9℃; Rate constant;
(Z)-2-Butene
590-18-1

(Z)-2-Butene

p-toluenesulfonyl chloride
98-59-9

p-toluenesulfonyl chloride

benzyl isothiocyanate
3173-56-6

benzyl isothiocyanate

A

4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

B

C28H31NO8S2

C28H31NO8S2

Conditions
ConditionsYield
Yield given. Multistep reaction. Yields of byproduct given;
thionyl chloride
7719-09-7

thionyl chloride

4-methoxybenzoic acid
100-09-4

4-methoxybenzoic acid

4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

phosphorus pentachloride
10026-13-8, 874483-75-7

phosphorus pentachloride

4-methoxybenzoic acid
100-09-4

4-methoxybenzoic acid

4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

oxalyl dichloride
79-37-8

oxalyl dichloride

sodium anisate

sodium anisate

4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

Conditions
ConditionsYield
With benzene
phosphorus pentachloride
10026-13-8, 874483-75-7

phosphorus pentachloride

4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

Conditions
ConditionsYield
hydroanisoin;
4-hydroxy-benzoic acid
99-96-7

4-hydroxy-benzoic acid

4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: KOH / ethanol / Heating
2: SOCl2
View Scheme
Multi-step reaction with 2 steps
1: KOH / ethanol
2: SOCl2
View Scheme
Multi-step reaction with 2 steps
1.1: potassium hydroxide
1.2: Reflux
2.1: thionyl chloride / Reflux
View Scheme
4-hydroxy-benzoic acid
99-96-7

4-hydroxy-benzoic acid

Nα-Fmoc-Nim-tert-butyloxycarbonyl-L-tryptophan 4-hydroxymethylphenoxy resin

Nα-Fmoc-Nim-tert-butyloxycarbonyl-L-tryptophan 4-hydroxymethylphenoxy resin

A

4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

B

aminoacyl chlorotrityl resin

aminoacyl chlorotrityl resin

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: KOH / ethanol
2: SOCl2
View Scheme
Multi-step reaction with 2 steps
1: alcohol; KOH
2: SOCl2
View Scheme
Ethyl 4-hydroxybenzoate
120-47-8

Ethyl 4-hydroxybenzoate

(+-)-methylphosphonic acid ethyl ester chloride

(+-)-methylphosphonic acid ethyl ester chloride

A

4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

B

aminoacyl chlorotrityl resin

aminoacyl chlorotrityl resin

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: NaOEt / 3 h / Heating
2: KOH / ethanol
3: SOCl2
View Scheme
ethyl 4-methoxybenzoate
94-30-4

ethyl 4-methoxybenzoate

A

4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

B

aminoacyl chlorotrityl resin

aminoacyl chlorotrityl resin

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: KOH / ethanol
2: SOCl2
View Scheme
4-hydroxy-benzoic acid
99-96-7

4-hydroxy-benzoic acid

source of vinyl group

source of vinyl group

A

4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

B

aminoacyl chlorotrityl resin

aminoacyl chlorotrityl resin

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: conc. H2SO4 / Heating
2: NaOEt / 3 h / Heating
3: KOH / ethanol
4: SOCl2
View Scheme
4-methoxyphenylacetamide
3424-93-9

4-methoxyphenylacetamide

4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 93 percent / TiCl4 / dioxane; H2O / 19 h / Heating
2: oxalyl chloride / CH2Cl2 / 0 - 20 °C
View Scheme
4-hydroxy-benzoic acid
99-96-7

4-hydroxy-benzoic acid

aqueous solution of pH 4,3

aqueous solution of pH 4,3

A

4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

B

hydrogen persulfide

hydrogen persulfide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
2: thionyl chloride / 2 h / Heating
View Scheme
methyl 4-methoxybenzoate
121-98-2

methyl 4-methoxybenzoate

A

4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

B

hydrogen persulfide

hydrogen persulfide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 81 percent / KOH / methanol; H2O / 4 h / Heating
2: thionyl chloride / 1 h / Heating
View Scheme
Multi-step reaction with 2 steps
1: 6percent aq. KOH
2: SOCl2
View Scheme
isobutylamine
78-81-9

isobutylamine

4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

N-isobutyl-4-methoxybenzamide
7464-51-9

N-isobutyl-4-methoxybenzamide

Conditions
ConditionsYield
With triethylamine In benzene100%
1,12-Diaminododecane
2783-17-7

1,12-Diaminododecane

4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

C28H40N2O4
27890-95-5

C28H40N2O4

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 2h; Inert atmosphere;100%
With potassium hydroxide In 1,2-dichloro-ethane
With potassium hydroxide
4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

tert-butylamine
75-64-9

tert-butylamine

N-tert-butyl-4-methoxybenzamide
19486-73-8

N-tert-butyl-4-methoxybenzamide

Conditions
ConditionsYield
With sodium hydroxide In dichloromethane100%
With dmap; sodium hydroxide In dichloromethane at 0 - 20℃;100%
In tetrahydrofuran at 0℃;86%
diphenylphosphinous acid methyl ester
4020-99-9

diphenylphosphinous acid methyl ester

4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

(diphenylphosphoryl)(4-methoxyphenyl)methanone
87361-23-7

(diphenylphosphoryl)(4-methoxyphenyl)methanone

Conditions
ConditionsYield
at 25℃;100%
In toluene at 60℃; for 2h; Michaelis-Arbuzov reaction;77%
N-methoxylamine hydrochloride
593-56-6

N-methoxylamine hydrochloride

4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

N-methoxy-4-methoxylbenzamide
24056-08-4

N-methoxy-4-methoxylbenzamide

Conditions
ConditionsYield
With pyridine In dichloromethane at 20℃; for 2h;100%
With sodium carbonate In water; benzene at 20℃; for 18h; Cooling;98%
With potassium carbonate In water; ethyl acetate at 0 - 20℃;98%
methyl 3,4-dihydro-1-methyl-β-carboline-3-carboxylate
51372-96-4

methyl 3,4-dihydro-1-methyl-β-carboline-3-carboxylate

4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

methyl 2-(4-methoxybenzoyl)-2,3,4,9-tetrahydro-1-methylene-1H-pyrido<3,4-b>indole-3-carboxylate
84576-15-8

methyl 2-(4-methoxybenzoyl)-2,3,4,9-tetrahydro-1-methylene-1H-pyrido<3,4-b>indole-3-carboxylate

Conditions
ConditionsYield
With triethylamine In benzene 1.) R.T., 2.) 50 deg C, 2 h.;100%
4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

diisopropylamine
108-18-9

diisopropylamine

N,N-diisopropyl-4-methoxybenzamide
79606-43-2

N,N-diisopropyl-4-methoxybenzamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 50℃; for 18h;100%
With triethylamine In dichloromethane at 0 - 20℃; for 12h;91%
With triethylamine In dichloromethane at 20℃; for 4h; Inert atmosphere;81%
4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

4-methoxybenzohydroxamic acid
10507-69-4

4-methoxybenzohydroxamic acid

Conditions
ConditionsYield
With hydroxylamine hydrochloride; sodium hydrogencarbonate In water; ethyl acetate at 20℃; for 0.0833333h;100%
With hydroxylamine hydrochloride; sodium hydrogencarbonate In water; ethyl acetate at 20℃; for 0.0833333h;95%
With hydroxylamine hydrochloride; potassium carbonate In water; ethyl acetate at 0 - 20℃; for 16h;56%
3-amino-2-methyl-4-oxoquinazoline
1898-06-2

3-amino-2-methyl-4-oxoquinazoline

4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

4-methoxy-N-(2-methyl-4-oxo-4H-quinazolin-3-yl)-benzamide
6761-15-5

4-methoxy-N-(2-methyl-4-oxo-4H-quinazolin-3-yl)-benzamide

Conditions
ConditionsYield
With pyridine In benzene for 2h; Heating;100%
4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

Potassium; 2-triisopropylsilanyloxy-butane-1-thiolate

Potassium; 2-triisopropylsilanyloxy-butane-1-thiolate

4-Methoxy-thiobenzoic acid S-(2-triisopropylsilanyloxy-butyl) ester

4-Methoxy-thiobenzoic acid S-(2-triisopropylsilanyloxy-butyl) ester

Conditions
ConditionsYield
In tetrahydrofuran at 0℃; for 2h;100%
4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

2-phenyl-2-propylamine
585-32-0

2-phenyl-2-propylamine

4-methoxy-N-(1-methyl-1-phenylethyl)benzamide
454479-63-1

4-methoxy-N-(1-methyl-1-phenylethyl)benzamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0℃; for 18h;100%
With triethylamine In dichloromethane for 12h;87%
In tetrahydrofuran at 0℃;84%
With triethylamine In dichloromethane Acylation;
4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

1-(2,5-Dichlorophenyl)-2,2-bis(methylsulfanyl)ethanone
171897-89-5

1-(2,5-Dichlorophenyl)-2,2-bis(methylsulfanyl)ethanone

4-methoxy-benzoic acid 1-(2,5-dichloro-phenyl)-2,2-bis-methylsulfanyl-vinyl ester

4-methoxy-benzoic acid 1-(2,5-dichloro-phenyl)-2,2-bis-methylsulfanyl-vinyl ester

Conditions
ConditionsYield
Stage #1: 1-(2,5-Dichlorophenyl)-2,2-bis(methylsulfanyl)ethanone With sodium hydride In tetrahydrofuran Metallation;
Stage #2: 4-methoxy-benzoyl chloride In tetrahydrofuran at 20℃; for 0.5h; Acylation;
100%
N-(p-methoxybenzyl)-N-tert-butylamine
22675-83-8

N-(p-methoxybenzyl)-N-tert-butylamine

4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

N-tert-butyl-4-methoxy-N-(4-methoxy-benzyl)-benzamide
335596-11-7

N-tert-butyl-4-methoxy-N-(4-methoxy-benzyl)-benzamide

Conditions
ConditionsYield
With sodium hydroxide In dichloromethane for 24h;100%
4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

N-tert-butylbenzylamine
3378-72-1

N-tert-butylbenzylamine

N-benzyl-N-tert-butyl-4-methoxy-benzamide
133587-81-2

N-benzyl-N-tert-butyl-4-methoxy-benzamide

Conditions
ConditionsYield
With sodium hydroxide In dichloromethane for 24h;100%
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