tribromo(3-bromopropyl)stannane

Base Information

• Chemical Name: tribromo(3-bromopropyl)stannane
• CAS No.: 61222-01-3
• Molecular Formula: C₃H₆Br₄Sn
• Molecular Weight: 480.407
• Mol file: 61222-01-3.mol

Synonyms:Tin,tribromo(1-bromopropyl)- (7CI); NSC 227318

Chemical Property of tribromo(3-bromopropyl)stannane

Chemical Property:

• Vapor Pressure: 0.00409mmHg at 25°C
• Boiling Point: 288.3°Cat760mmHg
• Flash Point: 128.1°C
• Density: g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of tribromo(3-bromopropyl)stannane

There total 2 articles about tribromo(3-bromopropyl)stannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

tin(II) bromide + 1,3-dibromo-propane (109-64-8) → Br3Sn(CH2)3Br (61222-01-3)

Guidance literature:

With triethylantimony; In neat (no solvent); (N2); std. Schlenk technique; according to Bulten E. J., et al., J. Organomet. Chem., 1976, 117, 329; suspn. of SnBr2, dibromopropane and Et3Sb was slowly warmed to 155°C within 45 min and stirred for 5 h; dibromopropane removed (vac.); distd.; elem. anal.;

DOI:10.1021/om0602005

Reference yield:

→ Br3Sn(CH2)3Br (61222-01-3)

Guidance literature:

SnBr2, Br(CH2)3Br, Et3Sb;

DOI:10.1016/S0022-328X(00)87210-1

upstream raw materials:

1,3-dibromo-propane