2,7-Dichloro-5-oxidophenazin-5-ium

Base Information

• Chemical Name: 2,7-Dichloro-5-oxidophenazin-5-ium
• CAS No.: 2680-66-2
• Molecular Formula: C12H6 Cl2 N2 O
• Molecular Weight: 265.098
• NSC Number: 202942
• DSSTox Substance ID: DTXSID10308286
• Nikkaji Number: J1.427.442A
• Wikidata: Q82056080
• Mol file: 2680-66-2.mol

Synonyms:2680-66-2;2,7-dichloro-5-oxidophenazin-5-ium;NSC202942;DTXSID10308286;NSC-202942

Chemical Property of 2,7-Dichloro-5-oxidophenazin-5-ium

Chemical Property:

• Vapor Pressure: 2.31E-08mmHg at 25°C
• Boiling Point: 464.5°C at 760 mmHg
• Flash Point: 234.7°C
• Density: 1.54g/cm³
• XLogP3: 2.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 0
• Exact Mass: 263.9857182
• Heavy Atom Count: 17
• Complexity: 292

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC2=C(C=C1Cl)[N+](=C3C=CC(=CC3=N2)Cl)[O-]

Technology Process of 2,7-Dichloro-5-oxidophenazin-5-ium

There total 4 articles about 2,7-Dichloro-5-oxidophenazin-5-ium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-chloro-aniline (106-47-8) + 4-chlorobenzonitrile (100-00-5) → 2,7-dichloro-phenazine 5-oxide (2680-66-2)

Guidance literature:

With sodium hydroxide; at 110 - 120 ℃;

Reference yield:

→ 2,7-dichloro-phenazine 5-oxide (2680-66-2)

Guidance literature:

With sulfuric acid; acetic acid; at 20 ℃;

Reference yield:

→ 2,7-dichloro-phenazine 5-oxide (2680-66-2)

Guidance literature:

With phosphorus pentachloride; trichlorophosphate; at 160 - 165 ℃;

DOI:10.1007/s12009-001-0007-z

upstream raw materials:

4-chloro-aniline

4-chlorobenzonitrile

Downstream raw materials:

2-Chlor-6-hydroxyphenazin-10-oxid