Cyclopentyl (6,11-dihydrodibenzo(b,e)thiepin-11-yl)carbamate

Base Information

Chemical Name:Cyclopentyl (6,11-dihydrodibenzo(b,e)thiepin-11-yl)carbamate
CAS No.:74797-22-1
Molecular Formula:C₂₀H₂₁NO₂S
Molecular Weight:339.458
Hs Code.:
DSSTox Substance ID:DTXSID80996316
Mol file:74797-22-1.mol

Synonyms:74797-22-1;BRN 4542296;VUFB-12444;Cyclopentyl (6,11-dihydrodibenzo(b,e)thiepin-11-yl)carbamate;cyclopentyl N-(6,11-dihydrobenzo[c][1]benzothiepin-11-yl)carbamate;Carbamic acid, (6,11-dihydrodibenzo(b,e)thiepin-11-yl)-, cyclopentyl ester;Oprea1_487343;cyclopentyl 6,11-dihydrodibenzo[b,e]thiepin-11-ylcarbamate;DTXSID80996316;LVAYCUHDBONTPY-UHFFFAOYSA-N;ZINC00347586;AKOS005066063;LS-49348;AE-641/30116060;Cyclopentyl hydrogen 6,11-dihydrodibenzo[b,e]thiepin-11-ylcarbonimidate

Suppliers and Price of Cyclopentyl (6,11-dihydrodibenzo(b,e)thiepin-11-yl)carbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Cyclopentyl (6,11-dihydrodibenzo(b,e)thiepin-11-yl)carbamate

Chemical Property:

Vapor Pressure:3.36E-10mmHg at 25°C
Boiling Point:501.8°C at 760 mmHg
Flash Point:257.3°C
PSA：67.12000
Density:1.26g/cm³
LogP:5.25490
XLogP3:4.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:339.12930009
Heavy Atom Count:24
Complexity:437

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCC(C1)OC(=O)NC2C3=CC=CC=C3CSC4=CC=CC=C24

Technology Process of Cyclopentyl (6,11-dihydrodibenzo(b,e)thiepin-11-yl)carbamate

There total 2 articles about Cyclopentyl (6,11-dihydrodibenzo(b,e)thiepin-11-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1745-46-6
6,11-dihydrodibenzo[b,e]thiepin-11-ol

: 4144-77-8
cyclopentyl carbamate

: 74797-22-1
(5,11-Dihydro-10-thia-dibenzo[a,d]cyclohepten-5-yl)-carbamic acid cyclopentyl ester

Guidance literature:: With toluene-4-sulfonic acid; In acetic acid; 1) 37 deg C, 6h; 2) room temp., overnight;
DOI:10.1135/cccc19800517

Reference yield:

: 96-41-3
Cyclopentanol

: 74797-22-1
(5,11-Dihydro-10-thia-dibenzo[a,d]cyclohepten-5-yl)-carbamic acid cyclopentyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / trifluoroacetic acid / benzene / 1) 30 min.(addition); 2) 52 h, room temp.

2: 97 percent / 4-toluenesulfonic acid / acetic acid / 1) 37 deg C, 6h; 2) room temp., overnight

With toluene-4-sulfonic acid; trifluoroacetic acid; In acetic acid; benzene;
DOI:10.1135/cccc19800517