N-(3-amino-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-2-chloroacetamide

Base Information

Chemical Name:N-(3-amino-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-2-chloroacetamide
CAS No.:30007-59-1
Molecular Formula:C₁₂H₉ClN₂O₃
Molecular Weight:264.668
Hs Code.:
Mol file:30007-59-1.mol

Synonyms:Acetamide,N-(3-amino-1,4-dihydro-1,4-dioxo-2-naphthyl)-2-chloro- (8CI); NSC 355045

Suppliers and Price of N-(3-amino-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-2-chloroacetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of N-(3-amino-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-2-chloroacetamide

Chemical Property:

Vapor Pressure:4.61E-09mmHg at 25°C
Boiling Point:471.5°Cat760mmHg
Flash Point:239°C
Density:1.49g/cm³

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-(3-amino-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-2-chloroacetamide

There total 4 articles about N-(3-amino-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-2-chloroacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 13755-95-8
2,3-diamino-1,4-naphthoquinone

: 79-04-9
chloroacetyl chloride

: 30007-59-1
N-(3-amino-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-2-chloroacetamide

Guidance literature:: 2,3-diamino-1,4-naphthoquinone; With pyridine; In chloroform; at 0 ℃; for 0.25h;

chloroacetyl chloride; In chloroform; at 0 - 20 ℃; for 6h;
DOI:10.1016/j.bioorg.2020.104441

Reference yield:

: 54010-92-3
NSC₁₃₀₄₄₀

: 30007-59-1
N-(3-amino-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-2-chloroacetamide

Guidance literature:: With 1,4-dioxane; ammonia;
DOI:10.1021/ja01645a028

Reference yield:

: 117-80-6
2,3-Dichloro-1,4-naphthoquinone

: 30007-59-1
N-(3-amino-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-2-chloroacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol; aqueous NH₃

2: HCl; xylene

3: dioxane; NH₃

With 1,4-dioxane; hydrogenchloride; ammonium hydroxide; ethanol; ammonia; xylene;
DOI:10.1021/ja01645a028