Hexanedioic acid, chloromethyl phenylmethyl ester

Base Information

Chemical Name:Hexanedioic acid, chloromethyl phenylmethyl ester
CAS No.:87343-30-4
Molecular Formula:C14H17ClO4
Molecular Weight:284.74
Hs Code.:
DSSTox Substance ID:DTXSID10444138

Synonyms:Benzyl chloromethyl adipate;Hexanedioic acid, chloromethyl phenylmethyl ester;87343-30-4;SCHEMBL10918679;DTXSID10444138;TZGBCSIGRNIPLC-UHFFFAOYSA-N

Suppliers and Price of Hexanedioic acid, chloromethyl phenylmethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Hexanedioic acid, chloromethyl phenylmethyl ester

Chemical Property:

XLogP3:2.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:10
Exact Mass:284.0815367
Heavy Atom Count:19
Complexity:275

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)COC(=O)CCCCC(=O)OCCl

Technology Process of Hexanedioic acid, chloromethyl phenylmethyl ester

There total 3 articles about Hexanedioic acid, chloromethyl phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 40542-90-3
adipic acid monobenzyl ester

: 87343-30-4
benzyl chloromethyl adipate

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / Cs₂CO₃ / dimethylformamide / 1.) room temperature, 30 min; 70 deg C, 15 min, 2.) room temperature, 3 h; 70 deg C, 15 min

2: 1.) SO₂Cl₂, 2.) cis-4-cyclohexene-1,2-dicarboxylic acid / 1.) CH₂Cl₂, room temperature, 1 h, 2.) 1 h

With sulfuryl dichloride; cis-1,2,3,6-tetrahydrophthalic acid; caesium carbonate; In N,N-dimethyl-formamide;
DOI:10.1021/jo971076p

Reference yield:

: 201210-69-7
Hexanedioic acid benzyl ester phenylsulfanylmethyl ester

: 87343-30-4
benzyl chloromethyl adipate

: (1R,2S)-4-Chloro-5-phenylsulfanyl-cyclohexane-1,2-dicarboxylic acid

Guidance literature:: With sulfuryl dichloride; cis-1,2,3,6-tetrahydrophthalic acid; Yield given. Multistep reaction; 1.) CH₂Cl₂, room temperature, 1 h, 2.) 1 h;
DOI:10.1021/jo971076p