Benzeneacetic acid, a-(phenylthio)-,2-(2,2-dichloroacetyl)hydrazide

Base Information

• Chemical Name: Benzeneacetic acid, a-(phenylthio)-,2-(2,2-dichloroacetyl)hydrazide
• CAS No.: 32121-57-6
• Molecular Formula: C₁₆H₁₄Cl₂N₂O₂S
• Molecular Weight: 369.271
• Mol file: 32121-57-6.mol

Synonyms:Hydrazine,1-(dichloroacetyl)-2-[phenyl(phenylthio)acetyl]- (8CI); NSC 148010

Chemical Property of Benzeneacetic acid, a-(phenylthio)-,2-(2,2-dichloroacetyl)hydrazide

Chemical Property:

• Boiling Point: 569°Cat760mmHg
• Flash Point: 297.9°C
• Density: 1.4g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzeneacetic acid, a-(phenylthio)-,2-(2,2-dichloroacetyl)hydrazide

There total 4 articles about Benzeneacetic acid, a-(phenylthio)-,2-(2,2-dichloroacetyl)hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bromo-phenyl-acetic acid methyl ester (37167-62-7,3042-81-7,61139-20-6) → Dichloro-acetic acid N'-(2-phenyl-2-phenylsulfanyl-acetyl)-hydrazide (32121-57-6)

Guidance literature:

Multi-step reaction with 3 steps

1: NaOMe

2: N₂H₄*H₂O

With sodium methylate; hydrazine hydrate;

Reference yield:

methyl α-phenyl-α-(phenylthio)acetate (51256-38-3) → Dichloro-acetic acid N'-(2-phenyl-2-phenylsulfanyl-acetyl)-hydrazide (32121-57-6)

Guidance literature:

Multi-step reaction with 2 steps

1: N₂H₄*H₂O

With hydrazine hydrate;

Reference yield:

thiophenol (108-98-5) → Dichloro-acetic acid N'-(2-phenyl-2-phenylsulfanyl-acetyl)-hydrazide (32121-57-6)

Guidance literature:

Multi-step reaction with 3 steps

1: NaOMe

2: N₂H₄*H₂O

With sodium methylate; hydrazine hydrate;

upstream raw materials:

dichloroacethyl chloride

phenyl-phenylsulfanyl-acetic acid hydrazide

bromo-phenyl-acetic acid methyl ester

methyl α-phenyl-α-(phenylthio)acetate

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