Benzoic acid, 4-(2-ethoxy-2-oxoethoxy)-3-nitro-, methyl ester

Base Information

Chemical Name:Benzoic acid, 4-(2-ethoxy-2-oxoethoxy)-3-nitro-, methyl ester
CAS No.:873852-15-4
Molecular Formula:C12H13NO7
Molecular Weight:283.238
Hs Code.:

Synonyms:methyl 4-ethoxycarbonylmethyloxy-3-nitrobenzoate;Benzoic acid,4-(2-ethoxy-2-oxoethoxy)-3-nitro-,methyl ester;

Suppliers and Price of Benzoic acid, 4-(2-ethoxy-2-oxoethoxy)-3-nitro-, methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzoic acid, 4-(2-ethoxy-2-oxoethoxy)-3-nitro-, methyl ester

Chemical Property:

PSA：107.65000
LogP:1.84650

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzoic acid, 4-(2-ethoxy-2-oxoethoxy)-3-nitro-, methyl ester

There total 3 articles about Benzoic acid, 4-(2-ethoxy-2-oxoethoxy)-3-nitro-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 99-42-3
methyl (4-hydroxy-3-nitro)benzoate

: 105-36-2
ethyl bromoacetate

: 873852-15-4
methyl 4-(2-ethoxy-2-oxoethoxy)-3-nitrobenzoate

Guidance literature:: methyl (4-hydroxy-3-nitro)benzoate; With potassium hydroxide; In ethanol; for 1h;

ethyl bromoacetate; In N,N-dimethyl-formamide; for 24h; Further stages.;
DOI:10.1021/jf062709g

Reference yield:

: 623-50-7
ethyl 2-hydroxyacetate

: 329-59-9
4-fluoro-3-nitro-benzoic acid methyl ester

: 873852-15-4
methyl 4-(2-ethoxy-2-oxoethoxy)-3-nitrobenzoate

Guidance literature:: With triethylamine; In acetonitrile; at 0 - 5 ℃; for 0.5h;
DOI:10.1016/j.ejmech.2020.112869

Reference yield:

: 616-82-0
3-nitro-4-hydroxybenzoic acid

: 873852-15-4
methyl 4-(2-ethoxy-2-oxoethoxy)-3-nitrobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid / Reflux

2: potassium carbonate / N,N-dimethyl-formamide / 8 h / 70 °C

With sulfuric acid; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2016.02.009