2,2'-Bipyridine, 5-[[2-[2-(2-bromoethoxy)ethoxy]ethoxy]methyl]-5'-[[2-[2-[2-[4-[tris[4-(1,1- dimethylethyl)phenyl]methyl]phenoxy]ethoxy]ethoxy]ethoxy]methyl]-

Base Information

Chemical Name:2,2'-Bipyridine, 5-[[2-[2-(2-bromoethoxy)ethoxy]ethoxy]methyl]-5'-[[2-[2-[2-[4-[tris[4-(1,1- dimethylethyl)phenyl]methyl]phenoxy]ethoxy]ethoxy]ethoxy]methyl]-
CAS No.:873865-97-5
Molecular Formula:C61H77BrN2O7
Molecular Weight:1030.2
Hs Code.:

2,2'-Bipyridine,
5-[[2-[2-(2-bromoethoxy)ethoxy]ethoxy]methyl]-5'-[[2-[2-[2-[4-[tris[4-(1,1-
dimethylethyl)phenyl]methyl]phenoxy]ethoxy]ethoxy]ethoxy]methyl]-

Synonyms:

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Chemical Property of 2,2'-Bipyridine, 5-[[2-[2-(2-bromoethoxy)ethoxy]ethoxy]methyl]-5'-[[2-[2-[2-[4-[tris[4-(1,1- dimethylethyl)phenyl]methyl]phenoxy]ethoxy]ethoxy]ethoxy]methyl]-

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Technology Process of 2,2'-Bipyridine, 5-[[2-[2-(2-bromoethoxy)ethoxy]ethoxy]methyl]-5'-[[2-[2-[2-[4-[tris[4-(1,1- dimethylethyl)phenyl]methyl]phenoxy]ethoxy]ethoxy]ethoxy]methyl]-

There total 6 articles about 2,2'-Bipyridine, 5-[[2-[2-(2-bromoethoxy)ethoxy]ethoxy]methyl]-5'-[[2-[2-[2-[4-[tris[4-(1,1- dimethylethyl)phenyl]methyl]phenoxy]ethoxy]ethoxy]ethoxy]methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 873865-95-3
5,5'-bis-{2-[2-(2-bromo-ethoxy)-ethoxy]-ethoxymethyl}-[2,2']bipyridinyl

: 143998-20-3
4-[tris-(4-tert-butylphenyl)methyl]phenol

: 873865-97-5
5'-{2-[2-(2-bromo-ethoxy)-ethoxy]-ethoxymethyl}-5-{2-[2-(2-{4-[tris-(4-tert-butyl-phenyl)-methyl]-phenoxy}-ethoxy)-ethoxy]-ethoxymethyl}-[2,2']bipyridinyl

Guidance literature:: 4-[tris-(4-tert-butylphenyl)methyl]phenol; With sodium hydride; In tetrahydrofuran; at 50 ℃; for 2h;

5,5'-bis-{2-[2-(2-bromo-ethoxy)-ethoxy]-ethoxymethyl}-[2,2']bipyridinyl; In tetrahydrofuran; at 50 ℃; for 24h;
DOI:10.1021/ol052051c

Reference yield:

: 873865-91-9
2-{2-[2-(5'-{2-[2-(2-hydroxy-ethoxy)-ethoxy]-ethoxymethyl}-[2,2']bipyridinyl-5-ylmethoxy)-ethoxy]-ethoxy}-ethanol

: 873865-97-5
5'-{2-[2-(2-bromo-ethoxy)-ethoxy]-ethoxymethyl}-5-{2-[2-(2-{4-[tris-(4-tert-butyl-phenyl)-methyl]-phenoxy}-ethoxy)-ethoxy]-ethoxymethyl}-[2,2']bipyridinyl

Guidance literature:: Multi-step reaction with 3 steps

1.1: Et₃N / CH₂Cl₂ / -5 - 20 °C

2.1: LiBr / acetone / 5 h / 20 °C

3.1: NaH / tetrahydrofuran / 2 h / 50 °C

3.2: 30 percent / tetrahydrofuran / 24 h / 50 °C

With sodium hydride; triethylamine; lithium bromide; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1021/ol052051c

Reference yield:

: 873865-93-1
methanesulfonic acid 2-{2-[2-(5'-{2-[2-(2-methanesulfonyloxy-ethoxy)-ethoxy]-ethoxymethyl}-[2,2']bipyridinyl-5-ylmethoxy)-ethoxy]-ethoxy}-ethyl ester

: 873865-97-5
5'-{2-[2-(2-bromo-ethoxy)-ethoxy]-ethoxymethyl}-5-{2-[2-(2-{4-[tris-(4-tert-butyl-phenyl)-methyl]-phenoxy}-ethoxy)-ethoxy]-ethoxymethyl}-[2,2']bipyridinyl

Guidance literature:: Multi-step reaction with 2 steps

1.1: LiBr / acetone / 5 h / 20 °C

2.1: NaH / tetrahydrofuran / 2 h / 50 °C

2.2: 30 percent / tetrahydrofuran / 24 h / 50 °C

With sodium hydride; lithium bromide; In tetrahydrofuran; acetone;
DOI:10.1021/ol052051c