Oxiranemethanol, 3-[(3E)-7-(octyloxy)-8-phenyl-3-octenyl]-, (2S,3S)-

Base Information

Chemical Name:Oxiranemethanol, 3-[(3E)-7-(octyloxy)-8-phenyl-3-octenyl]-, (2S,3S)-
CAS No.:873925-46-3
Molecular Formula:C25H40O3
Molecular Weight:388.591
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Oxiranemethanol, 3-[(3E)-7-(octyloxy)-8-phenyl-3-octenyl]-, (2S,3S)-

Chemical Property:

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Technology Process of Oxiranemethanol, 3-[(3E)-7-(octyloxy)-8-phenyl-3-octenyl]-, (2S,3S)-

There total 8 articles about Oxiranemethanol, 3-[(3E)-7-(octyloxy)-8-phenyl-3-octenyl]-, (2S,3S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 451503-10-9
(2E,6E)-10-Octyloxy-11-phenyl-undeca-2,6-dien-1-ol

: 873925-46-3
[(2S,3S)-3-((E)-7-Octyloxy-8-phenyl-oct-3-enyl)-oxiranyl]-methanol

Guidance literature:: With titanium(IV) isopropylate; tert.-butylhydroperoxide; 4 A molecular sieve; L-(+)-diisopropyl tartrate; In dichloromethane;
DOI:10.1021/ol0261074

Reference yield:

: 451503-08-5
4-octyloxy-5-phenyl-pentanal

: 873925-46-3
[(2S,3S)-3-((E)-7-Octyloxy-8-phenyl-oct-3-enyl)-oxiranyl]-methanol

Guidance literature:: Multi-step reaction with 5 steps

1.1: tetrahydrofuran

2.1: 75 percent / propionic acid / xylene

3.1: DIBAL-H / CH₂Cl₂

3.2: 87 percent / CH₂Cl₂

4.1: 81 percent / DIBAL-H / CH₂Cl₂

5.1: 93 percent / t-BuOOH; (i-PrO)4Ti; 4 Angstroem molecular sieves / (+)-diisopropyl tartrate / CH₂Cl₂

With titanium(IV) isopropylate; tert.-butylhydroperoxide; 4 A molecular sieve; diisobutylaluminium hydride; propionic acid; L-(+)-diisopropyl tartrate; In tetrahydrofuran; dichloromethane; xylene; 5.1: Sharpless epoxidation;
DOI:10.1021/ol0261074

Reference yield:

: 345895-23-0
(2-octyloxy-hex-5-enyl)-benzene

: 873925-46-3
[(2S,3S)-3-((E)-7-Octyloxy-8-phenyl-oct-3-enyl)-oxiranyl]-methanol

Guidance literature:: Multi-step reaction with 6 steps

1.1: O₃ / CH₂Cl₂

1.2: Ph₃P / CH₂Cl₂

2.1: tetrahydrofuran

3.1: 75 percent / propionic acid / xylene

4.1: DIBAL-H / CH₂Cl₂

4.2: 87 percent / CH₂Cl₂

5.1: 81 percent / DIBAL-H / CH₂Cl₂

6.1: 93 percent / t-BuOOH; (i-PrO)4Ti; 4 Angstroem molecular sieves / (+)-diisopropyl tartrate / CH₂Cl₂

With titanium(IV) isopropylate; tert.-butylhydroperoxide; 4 A molecular sieve; diisobutylaluminium hydride; ozone; propionic acid; L-(+)-diisopropyl tartrate; In tetrahydrofuran; dichloromethane; xylene; 6.1: Sharpless epoxidation;
DOI:10.1021/ol0261074