(1E,2E)-3,8-bis(4-methoxyphenyl)-4,5,6,7-tetrahydrodiazocine

Base Information

Chemical Name:(1E,2E)-3,8-bis(4-methoxyphenyl)-4,5,6,7-tetrahydrodiazocine
CAS No.:76907-95-4
Molecular Formula:C20H22N2O2
Molecular Weight:322.4009
Hs Code.:
NSC Number:518683
DSSTox Substance ID:DTXSID20430461

Synonyms:NSC518683;76907-95-4;DTXSID20430461;NSC-518683

Suppliers and Price of (1E,2E)-3,8-bis(4-methoxyphenyl)-4,5,6,7-tetrahydrodiazocine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of (1E,2E)-3,8-bis(4-methoxyphenyl)-4,5,6,7-tetrahydrodiazocine

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:446.5°Cat760mmHg
Flash Point:180°C
Density:1.11g/cm³
XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:322.168127949
Heavy Atom Count:24
Complexity:403

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=C1)C2=NN=C(CCCC2)C3=CC=C(C=C3)OC
Isomeric SMILES:COC1=CC=C(C=C1)/C/2=N/N=C(\CCCC2)/C3=CC=C(C=C3)OC

Technology Process of (1E,2E)-3,8-bis(4-methoxyphenyl)-4,5,6,7-tetrahydrodiazocine

There total 3 articles about (1E,2E)-3,8-bis(4-methoxyphenyl)-4,5,6,7-tetrahydrodiazocine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 4280-49-3
1,6-bis(4-methoxyphenyl)hexa-1,6-dione

: 76907-95-4
(1E,2E)-3,8-bis(4-methoxyphenyl)-4,5,6,7-tetrahydro-1,2-diazocine

Guidance literature:: With hydrazine hydrate; acetic acid; In ethanol; at 55 ℃; for 12h; Sealed tube; Inert atmosphere;
DOI:10.1021/acs.orglett.0c00967

Reference yield:

: 15973-65-6
1-(4-methoxyphenyl)cyclopropan-1-ol

: 76907-95-4
(1E,2E)-3,8-bis(4-methoxyphenyl)-4,5,6,7-tetrahydro-1,2-diazocine

Guidance literature:: Multi-step reaction with 2 steps

1: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; silver carbonate / 2,2,2-trifluoroethanol / 0.25 h / 20 °C / Schlenk technique; Sealed tube; Inert atmosphere

2: hydrazine hydrate; acetic acid / ethanol / 12 h / 55 °C / Sealed tube; Inert atmosphere

With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; hydrazine hydrate; acetic acid; silver carbonate; In ethanol; 2,2,2-trifluoroethanol;
DOI:10.1021/acs.orglett.0c00967