2,6-Dimethyl-4-(phenylazo)benzenamine

Base Information

• Chemical Name: 2,6-Dimethyl-4-(phenylazo)benzenamine
• CAS No.: 41165-12-2
• Molecular Formula: C14H15N3
• Molecular Weight: 225.289
• Hs Code.: 2927000090
• Mol file: 41165-12-2.mol

Synonyms:2,6-dimethyl-4-[(e)-phenyldiazenyl]aniline;5-Benzolazo-2-amino-m-xylol;4-Amino-3.5-dimethyl-azobenzol;Benzenamine, 2,6-dimethyl-4-(phenylazo)-;2,6-dimethyl-4-(phenylazo)-benzenamine;2,6-dimethyl-4-phenylazo-aniline;Benzol-azo-vic.-m-xylidin;

Chemical Property of 2,6-Dimethyl-4-(phenylazo)benzenamine

Chemical Property:

• Vapor Pressure: 8.25E-07mmHg at 25°C
• Boiling Point: 406.2°Cat760mmHg
• Flash Point: 199.5°C
• PSA: 50.74000
• Density: 1.09g/cm³
• LogP: 4.88220

Purity/Quality:

99% ^*data from raw suppliers

4-AMINO-3,5-DIMETHYLAZOBENZENE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of 2,6-Dimethyl-4-(phenylazo)benzenamine

There total 3 articles about 2,6-Dimethyl-4-(phenylazo)benzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

aniline (62-53-3) + 2,6-dimethylaniline (87-62-7) → (E)-2,6-dimethyl-4-(phenyldiazenyl)aniline (41165-12-2)

Guidance literature:

aniline; With hydrogenchloride; In water; at 0 - 5 ℃; for 0.333333h;

With sodium nitrite; In water; at 0 - 5 ℃; for 0.5h;

2,6-dimethylaniline; With hydrogenchloride; In water; at 5 ℃; for 6h;

DOI:10.1002/chem.201905161

Reference yield:

benzenediazonium (2684-02-8) + 2,6-dimethylaniline (87-62-7) → (E)-2,6-dimethyl-4-(phenyldiazenyl)aniline (41165-12-2)

Guidance literature:

With ethanol;

Reference yield:

benzene diazonium chloride (100-34-5) + 2,6-dimethylaniline (87-62-7) → (E)-2,6-dimethyl-4-(phenyldiazenyl)aniline (41165-12-2)

Guidance literature:

With hydrogenchloride;

upstream raw materials:

benzenediazonium

2,6-dimethylaniline

benzene diazonium chloride

aniline

Downstream raw materials:

acetic acid-(2,6,N-trimethyl-4-phenylazo-anilide)