N-Isopropyl-2,3-xylidine

Base Information

• Chemical Name: N-Isopropyl-2,3-xylidine
• CAS No.: 63114-76-1
• Molecular Formula: C11H17N
• Molecular Weight: 163.263
• Hs Code.: 2921430090
• European Community (EC) Number: 263-866-0
• DSSTox Substance ID: DTXSID90212453
• Nikkaji Number: J307.199E
• Wikidata: Q83087588
• Mol file: 63114-76-1.mol

Synonyms:N-Isopropyl-2,3-xylidine;63114-76-1;EINECS 263-866-0;2,3-dimethyl-N-(propan-2-yl)aniline;N-ISOPROPYL-2,3-DIMETHYLANILINE;SCHEMBL10393919;DTXSID90212453;IUEHLAXLHVYGLI-UHFFFAOYSA-N;AKOS000243122;2,3-Dimethyl-N-(1-methylethyl)benzenamine;CS-0274526;EN300-164248

Chemical Property of N-Isopropyl-2,3-xylidine

Chemical Property:

• Vapor Pressure: 0.0131mmHg at 25°C
• Boiling Point: 259.3°Cat760mmHg
• Flash Point: 110.5°C
• PSA: 12.03000
• Density: 0.933g/cm³
• LogP: 3.19670
• XLogP3: 3.4
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 163.136099547
• Heavy Atom Count: 12
• Complexity: 131

Purity/Quality:

98%Min ^*data from raw suppliers

AS000278:(2,3-Dimethyl-phenyl)-isopropyl-amine 96 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=C(C(=CC=C1)NC(C)C)C

Technology Process of N-Isopropyl-2,3-xylidine

There total 2 articles about N-Isopropyl-2,3-xylidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-bromo-o-xylene (583-71-1) + isopropylamine (75-31-0) → N-isopropyl-2,3-xylidine (63114-76-1) + N-(1-methylethyl)-3,4-dimethyl-aniline (105336-21-8)

Guidance literature:

With potassium amide; for 2h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Heating;

DOI:10.1021/jo00376a020

Reference yield:

→ N-isopropyl-2,3-xylidine (63114-76-1) + 2,3-Dimethylaniline (87-59-2)

Guidance literature:

Reference yield:

N-isopropyl-2,3-xylidine (63114-76-1) + chloroacetyl chloride (79-04-9) → 2-chloro-2',3'-dimethyl-N-(isopropyl)acetanilide (63114-77-2,73468-30-1,73560-72-2)

Guidance literature:

In pentane; benzene;

upstream raw materials:

4-bromo-o-xylene

isopropylamine

Downstream raw materials:

2-chloro-2',3'-dimethyl-N-(isopropyl)acetanilide

Refernces

• 1、 -. "2-Chloro-N-isopropyl-2',3'-dimethylacetanilide as a herbicidal agent". . . Retrieved 2008/06/13.