ethyl 5-acetoxy-6-broMo-2-(broMoMethyl)-1-cyclopropyl-1H-indole-3-carboxylate

Base Information

Chemical Name:ethyl 5-acetoxy-6-broMo-2-(broMoMethyl)-1-cyclopropyl-1H-indole-3-carboxylate
CAS No.:874595-64-9
Molecular Formula:C17H17Br2NO4
Molecular Weight:459.12900
Hs Code.:
Mol file:874595-64-9.mol

Synonyms:ethyl 5-acetoxy-6-bromo-2-bromomethyl-1-cylopropyl-1H-indole-3-carboxylate;

Suppliers and Price of ethyl 5-acetoxy-6-broMo-2-(broMoMethyl)-1-cyclopropyl-1H-indole-3-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemicals and raw materials
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Total 3 raw suppliers

Chemical Property of ethyl 5-acetoxy-6-broMo-2-(broMoMethyl)-1-cyclopropyl-1H-indole-3-carboxylate

Chemical Property:

PSA：57.53000
LogP:4.73560

Purity/Quality:: 97-99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of ethyl 5-acetoxy-6-broMo-2-(broMoMethyl)-1-cyclopropyl-1H-indole-3-carboxylate

There total 4 articles about ethyl 5-acetoxy-6-broMo-2-(broMoMethyl)-1-cyclopropyl-1H-indole-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 383402-59-3
5-acetoxy-1-cyclopropyl-2-methyl-1H-indole-3-carboxylic acid ethyl ester

: 874595-64-9
5-acetoxy-6-bromo-2-bromomethyl-1-cyclopropyl-1H-indole-3-carboxylic acid ethyl ester

Guidance literature:: With bromine; In tetrachloromethane; Heating;
DOI:10.1007/s11094-015-1244-6

Reference yield:

: 301173-79-5
ethyl 1-cyclopropyl-5-hydroxy-2-methylindole-3-carboxylate

: 874595-64-9
5-acetoxy-6-bromo-2-bromomethyl-1-cyclopropyl-1H-indole-3-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine

2: bromine / tetrachloromethane / Heating

With pyridine; bromine; In tetrachloromethane;
DOI:10.1007/s11094-015-1244-6

Reference yield:

: 213454-27-4
3-cyclopropylamino-but-2-enoic acid ethyl ester

: 874595-64-9
5-acetoxy-6-bromo-2-bromomethyl-1-cyclopropyl-1H-indole-3-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1,2-dichloro-ethane / 8 h / 60 °C / Heating / reflux

2: pyridine / acetone / 4 h / 20 - 30 °C

3: bromine / dibenzoyl peroxide / tetrachloromethane / 5 h / Heating / reflux

With pyridine; bromine; dibenzoyl peroxide; In tetrachloromethane; 1,2-dichloro-ethane; acetone;