2-Oxazolidinone, 3-[[[(1S,2R)-2-[(4-methoxyphenyl)methoxy]-1-methyl-1-[2-[[tris(1-methyl ethyl)silyl]oxy]ethyl]-4-pentenyl]oxy]acetyl]-4-(1-methylethyl)-, (4S)-

Base Information

Chemical Name:2-Oxazolidinone, 3-[[[(1S,2R)-2-[(4-methoxyphenyl)methoxy]-1-methyl-1-[2-[[tris(1-methyl ethyl)silyl]oxy]ethyl]-4-pentenyl]oxy]acetyl]-4-(1-methylethyl)-, (4S)-
CAS No.:874660-21-6
Molecular Formula:C33H55NO7Si
Molecular Weight:605.888
Hs Code.:

2-Oxazolidinone,
3-[[[(1S,2R)-2-[(4-methoxyphenyl)methoxy]-1-methyl-1-[2-[[tris(1-methyl
ethyl)silyl]oxy]ethyl]-4-pentenyl]oxy]acetyl]-4-(1-methylethyl)-, (4S)-

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Oxazolidinone, 3-[[[(1S,2R)-2-[(4-methoxyphenyl)methoxy]-1-methyl-1-[2-[[tris(1-methyl ethyl)silyl]oxy]ethyl]-4-pentenyl]oxy]acetyl]-4-(1-methylethyl)-, (4S)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
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Technology Process of 2-Oxazolidinone, 3-[[[(1S,2R)-2-[(4-methoxyphenyl)methoxy]-1-methyl-1-[2-[[tris(1-methyl ethyl)silyl]oxy]ethyl]-4-pentenyl]oxy]acetyl]-4-(1-methylethyl)-, (4S)-

There total 9 articles about 2-Oxazolidinone, 3-[[[(1S,2R)-2-[(4-methoxyphenyl)methoxy]-1-methyl-1-[2-[[tris(1-methyl ethyl)silyl]oxy]ethyl]-4-pentenyl]oxy]acetyl]-4-(1-methylethyl)-, (4S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₂H₅₄O₇Si

: 17016-83-0
(4S)-4-isopropyl-1,3-oxazolidin-2-one

: 874660-21-6
(S)-4-Isopropyl-3-{2-[(1S,2R)-2-(4-methoxy-benzyloxy)-1-methyl-1-(2-triisopropylsilanyloxy-ethyl)-pent-4-enyloxy]-acetyl}-oxazolidin-2-one

Guidance literature:: (4S)-4-isopropyl-1,3-oxazolidin-2-one; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.333333h;

C₃₂H₅₄O₇Si; In tetrahydrofuran; hexane; at -78 - 0 ℃; for 1h;
DOI:10.1021/ol0526625

Reference yield:

: 874660-41-0
(R)-4-(4-Methoxy-benzyloxy)-hept-6-ene-1,3-diol

: 874660-21-6
(S)-4-Isopropyl-3-{2-[(1S,2R)-2-(4-methoxy-benzyloxy)-1-methyl-1-(2-triisopropylsilanyloxy-ethyl)-pent-4-enyloxy]-acetyl}-oxazolidin-2-one

Guidance literature:: Multi-step reaction with 6 steps

1.1: 99 percent / imidazole / dimethylformamide / 0 - 20 °C

2.1: 96 percent / pyridine; Dess-Martin periodinane / CH₂Cl₂ / 1 h

3.1: 95 percent / tetrahydrofuran; diethyl ether / -78 °C

4.1: 73 percent / sodium hydride / tetrahydrofuran; dimethylformamide / 0 - 20 °C

5.1: triethylamine / tetrahydrofuran / -78 - 0 °C

6.1: n-butyl lithium / tetrahydrofuran; hexane / 0.33 h / -78 °C

6.2: 40 g / tetrahydrofuran; hexane / 1 h / -78 - 0 °C

With pyridine; 1H-imidazole; n-butyllithium; sodium hydride; Dess-Martin periodane; triethylamine; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol0526625

Reference yield:

: 874660-17-0
3-hydroxy-4-(4-methoxy-benzyloxy)-hept-6-enoic acid tert-butyl ester

: 874660-21-6
(S)-4-Isopropyl-3-{2-[(1S,2R)-2-(4-methoxy-benzyloxy)-1-methyl-1-(2-triisopropylsilanyloxy-ethyl)-pent-4-enyloxy]-acetyl}-oxazolidin-2-one

Guidance literature:: Multi-step reaction with 7 steps

1.1: 92 percent / lithium aluminum hydride / diethyl ether / 1.5 h / 0 °C

2.1: 99 percent / imidazole / dimethylformamide / 0 - 20 °C

3.1: 96 percent / pyridine; Dess-Martin periodinane / CH₂Cl₂ / 1 h

4.1: 95 percent / tetrahydrofuran; diethyl ether / -78 °C

5.1: 73 percent / sodium hydride / tetrahydrofuran; dimethylformamide / 0 - 20 °C

6.1: triethylamine / tetrahydrofuran / -78 - 0 °C

7.1: n-butyl lithium / tetrahydrofuran; hexane / 0.33 h / -78 °C

7.2: 40 g / tetrahydrofuran; hexane / 1 h / -78 - 0 °C

With pyridine; 1H-imidazole; lithium aluminium tetrahydride; n-butyllithium; sodium hydride; Dess-Martin periodane; triethylamine; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol0526625