Methanone, phenyl[6-(2-propenyloxy)-2-naphthalenyl]-

Base Information

Chemical Name:Methanone, phenyl[6-(2-propenyloxy)-2-naphthalenyl]-
CAS No.:874988-41-7
Molecular Formula:C20H16O2
Molecular Weight:288.346
Hs Code.:

Synonyms:

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Chemical Property of Methanone, phenyl[6-(2-propenyloxy)-2-naphthalenyl]-

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Technology Process of Methanone, phenyl[6-(2-propenyloxy)-2-naphthalenyl]-

There total 2 articles about Methanone, phenyl[6-(2-propenyloxy)-2-naphthalenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 52222-87-4
6-Benzoyl-2-naphthol

: 106-95-6
allyl bromide

: 874988-41-7
(6-allyloxy-naphthalen-2-yl)-phenyl-methanone

Guidance literature:: 6-Benzoyl-2-naphthol; With potassium hydroxide; In dimethyl sulfoxide; at 20 ℃; for 0.5h;

allyl bromide; In dimethyl sulfoxide; at 20 ℃; for 2h;
DOI:10.1021/jm0510373

Reference yield:

: 100-52-7
benzaldehyde

: 111359-65-0
6-Bromo-2-(2-propenyloxy)naphthalene

: 874988-41-7
(6-allyloxy-naphthalen-2-yl)-phenyl-methanone

Guidance literature:: 6-Bromo-2-(2-propenyloxy)naphthalene; With iodine; magnesium; In tetrahydrofuran; for 1h; Inert atmosphere;

benzaldehyde; In tetrahydrofuran; for 3h; Inert atmosphere;

With dipyridinium dichromate; In dichloromethane; for 4h; Inert atmosphere;
DOI:10.1021/jm801594x

Reference yield:

: 874988-41-7
(6-allyloxy-naphthalen-2-yl)-phenyl-methanone

: 874988-15-5
(6-hydroxy-5-propyl-naphthalen-2-yl)-phenyl-methanone

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / 1,2-dichloro-benzene / 0.25 h / 250 °C / microwave irradiation

2: 97 percent / H₂ / Pd/C / ethyl acetate / 2 h / 2280 Torr

With hydrogen; palladium on activated charcoal; In ethyl acetate; 1,2-dichloro-benzene; 1: Claisen rearrangement;
DOI:10.1021/jm0510373