METHYL 5-HYDROXY-2-METHOXYBENZOATE

Base Information

• Chemical Name: METHYL 5-HYDROXY-2-METHOXYBENZOATE
• CAS No.: 87513-63-1
• Molecular Formula: C9H10O4
• Molecular Weight: 182.176
• Hs Code.: 2918990090
• Mol file: 87513-63-1.mol

Synonyms:Benzoic acid,5-hydroxy-2-methoxy-,methyl ester;5-Hydroxy-2-methoxybenzoesaeure-methylester;methyl 2-methoxy-5-hydroxybenzoate;

Chemical Property of METHYL 5-HYDROXY-2-METHOXYBENZOATE

Chemical Property:

• Vapor Pressure: 9.99E-05mmHg at 25°C
• Boiling Point: 328.3oC at 760 mmHg
• Flash Point: 133.1oC
• PSA: 55.76000
• Density: 1.216g/cm3
• LogP: 1.18740

Purity/Quality:

99% ^*data from raw suppliers

methyl5-hydroxy-2-methoxybenzoate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of METHYL 5-HYDROXY-2-METHOXYBENZOATE

There total 14 articles about METHYL 5-HYDROXY-2-METHOXYBENZOATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

5-Benzyloxy-2-methoxybenzoesaeure-methylester (52329-04-1) → 5-Hydroxy-2-methoxybenzoesaeure-methylester (87513-63-1)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In ethanol; at 20 ℃; for 5h; under 1913.5 Torr; Inert atmosphere;

DOI:10.1021/jm5019252

Reference yield: 85.0%

C21H13F4O3S2(1+)*BF4(1-) → 5-Hydroxy-2-methoxybenzoesaeure-methylester (87513-63-1)

Guidance literature:

With copper(I) oxide; [4,4′-bis(1,1-dimethylethyl)-2,2′-bipyridine-N1,N1′]bis{3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-κN]phenyl-κC}iridium(III) hexafluorophosphate; water; butane-2,3-dione dioxime; In acetonitrile; at 30 ℃; for 16h; Irradiation; Inert atmosphere;

DOI:10.1002/anie.201908718

Reference yield: 50.0%

methyl 2-methoxy-5-pivaloyloxybenzoate (845307-14-4) → 5-Hydroxy-2-methoxybenzoesaeure-methylester (87513-63-1)

Guidance literature:

With potassium carbonate; In methanol; at 20 ℃; for 3h;

DOI:10.1515/znb-2004-0714

upstream raw materials:

5-Benzyloxy-2-methoxybenzoesaeure-methylester

5-Allyloxy-2-methoxy-benzoic acid methyl ester

diazomethane

2,5-dihydroxybenzoic acid.

Downstream raw materials:

5-Hydroxy-2-methoxybenzylalkohol

2-methoxy-5-hydroxybenzoic acid

cis-3-(3-Cyanmethyl-4-methoxyphenoxy)prolin

trans-3-(3-Cyanmethyl-4-methoxyphenoxy)prolin

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