(Hexane-1,6-diyl)bis[(6-chlorohexyl)(diphenyl)stannane]

Base Information

Chemical Name:(Hexane-1,6-diyl)bis[(6-chlorohexyl)(diphenyl)stannane]
CAS No.:87518-52-3
Molecular Formula:C42H56Cl2Sn2
Molecular Weight:869.233
Hs Code.:
DSSTox Substance ID:DTXSID60531224
Wikidata:Q82402923

Synonyms:87518-52-3;(Hexane-1,6-diyl)bis[(6-chlorohexyl)(diphenyl)stannane];DTXSID60531224

Suppliers and Price of (Hexane-1,6-diyl)bis[(6-chlorohexyl)(diphenyl)stannane]

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of (Hexane-1,6-diyl)bis[(6-chlorohexyl)(diphenyl)stannane]

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:23
Exact Mass:868.17972
Heavy Atom Count:46
Complexity:636

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)[Sn](CCCCCCCl)(CCCCCC[Sn](CCCCCCCl)(C2=CC=CC=C2)C3=CC=CC=C3)C4=CC=CC=C4

Technology Process of (Hexane-1,6-diyl)bis[(6-chlorohexyl)(diphenyl)stannane]

There total 1 articles about (Hexane-1,6-diyl)bis[(6-chlorohexyl)(diphenyl)stannane] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 87518-47-6
1,6-bis(bromodiphenylstannyl)hexane

: 361541-51-7
(6-chlorohexyl)magnesium bromide

: 87518-52-3
1,20-dichloro-7,7,13,13-tetraphenyl-7,13-distannaeicosane

Guidance literature:: With magnesium; In tetrahydrofuran; (N2); to suspn. of Mg at -10°C added over 40 min BrMg(CH2)6Cl soln., stirred for 30 min at 25°C and 60 min at 0°C, dilutedwith THF, added over 1.5 h soln. of Sn compd. at 0°C, warmed slowly, reacted for 7 h at 25°C; quenched with satd. aq. NH4Cl, aq. layer extd. (ether), combined org. layers washed (satd. aq. NaCl), dried (MgSO4), concd. (vac.), chromd. (MeCN/THF);
DOI:10.1021/om00079a003

Reference yield: 33.0%

: 87518-52-3
1,20-dichloro-7,7,13,13-tetraphenyl-7,13-distannaeicosane

: (C₆H₅)2Sn(Li)(CH₂)6Sn(Li)(C₆H₅)2

: 87518-40-9
1,1,8,8,15,15,22,22-octaphenyl-1,8,15,22-tetrastannacyclooctacosane

Guidance literature:: In tetrahydrofuran; (N2); soln. of dilithium compd. added over 2 h to soln. of dichloro-compd. at 0°C, allowed to warm to room temp., stirred for 18 h; satd. aq. NH4Cl added at 0°C, aq. layer extd. (ether), combined ethereal solns. washed (satd. aq. NaCl), dried (MgSO4), filtered, concd., chromd., recrystd. (hexane/ether); elem. anal.;
DOI:10.1021/om00079a003