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Acetic acid, (phenylthio)-, 8-hydroxy-3,7-dimethyl-2,6-octadienyl ester, (E,E)-

Base Information
  • Chemical Name:Acetic acid, (phenylthio)-, 8-hydroxy-3,7-dimethyl-2,6-octadienyl ester, (E,E)-
  • CAS No.:87519-22-0
  • Molecular Formula:C18H24O3S
  • Molecular Weight:320.453
  • Hs Code.:
Acetic acid, (phenylthio)-, 8-hydroxy-3,7-dimethyl-2,6-octadienyl ester,
(E,E)-

Synonyms:

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Chemical Property of Acetic acid, (phenylthio)-, 8-hydroxy-3,7-dimethyl-2,6-octadienyl ester, (E,E)-
Chemical Property:
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SDS file from LookChem

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Technology Process of Acetic acid, (phenylthio)-, 8-hydroxy-3,7-dimethyl-2,6-octadienyl ester, (E,E)-

There total 3 articles about Acetic acid, (phenylthio)-, 8-hydroxy-3,7-dimethyl-2,6-octadienyl ester, (E,E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 2 steps
1: 99.3 percent / pyridine / CH2Cl2 / 3 h
2: 1.) SeO2, 2.) cyanoborohydride / 1.) pyridine, 95percent ethanol, reflux, 4.5 h, 2.) THF, pH 3, 1 h, 0 deg C then 23 deg C, 18 h
With pyridine; selenium(IV) oxide; cyanoborane; In dichloromethane;
DOI:10.1021/jo00173a043
Guidance literature:
Multi-step reaction with 2 steps
1: 99.3 percent / pyridine / CH2Cl2 / 3 h
2: 1.) SeO2, 2.) cyanoborohydride / 1.) pyridine, 95percent ethanol, reflux, 4.5 h, 2.) THF, pH 3, 1 h, 0 deg C then 23 deg C, 18 h
With pyridine; selenium(IV) oxide; cyanoborane; In dichloromethane;
DOI:10.1021/jo00173a043
Guidance literature:
With selenium(IV) oxide; cyanoborane; Yield given. Multistep reaction; 1.) pyridine, 95percent ethanol, reflux, 4.5 h, 2.) THF, pH 3, 1 h, 0 deg C then 23 deg C, 18 h;
DOI:10.1021/jo00173a043
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