Technology Process of Benzoic acid, 4,4'-[(6-bromo-1-oxohexyl)imino]bis-, dimethyl ester
There total 4 articles about Benzoic acid, 4,4'-[(6-bromo-1-oxohexyl)imino]bis-, dimethyl ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
4-[(4-(methoxycarbonyl)phenyl)amino]benzoic acid methyl ester;
With
sodium hydride;
In
dibutyl ether;
at 20 ℃;
for 2h;
6-bromohexanoyl chloride;
In
dibutyl ether;
for 4h;
Heating;
DOI:10.1021/jm060468y
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: copper (I) iodide; K3PO4; trans-1,2-cyclohexanediamine / dibutyl ether / 5 h / Heating
1.2: sodium methoxide / methanol / 1.5 h / Heating
2.1: sodium hydride / dibutyl ether / 2 h / 20 °C
2.2: 88 percent / dibutyl ether / 4 h / Heating
With
potassium phosphate; copper(l) iodide; (S,S)-1,2-diaminocyclohexane; sodium hydride;
In
dibutyl ether;
DOI:10.1021/jm060468y
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: copper (I) iodide; K3PO4; trans-1,2-cyclohexanediamine / dibutyl ether / 5 h / Heating
1.2: sodium methoxide / methanol / 1.5 h / Heating
2.1: sodium hydride / dibutyl ether / 2 h / 20 °C
2.2: 88 percent / dibutyl ether / 4 h / Heating
With
potassium phosphate; copper(l) iodide; (S,S)-1,2-diaminocyclohexane; sodium hydride;
In
dibutyl ether;
DOI:10.1021/jm060468y
