Benzoic acid, 2-hydroxy-3-methyl-6-(3-methyl-4-oxobutyl)-, phenylmethyl ester, (S)-

Base Information

Chemical Name:Benzoic acid, 2-hydroxy-3-methyl-6-(3-methyl-4-oxobutyl)-, phenylmethyl ester, (S)-
CAS No.:87598-75-2
Molecular Formula:C₂₀H₂₂O₄
Molecular Weight:326.392
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzoic acid, 2-hydroxy-3-methyl-6-(3-methyl-4-oxobutyl)-, phenylmethyl ester, (S)-

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of Benzoic acid, 2-hydroxy-3-methyl-6-(3-methyl-4-oxobutyl)-, phenylmethyl ester, (S)-

There total 6 articles about Benzoic acid, 2-hydroxy-3-methyl-6-(3-methyl-4-oxobutyl)-, phenylmethyl ester, (S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 87598-77-4
1-[(tert-butyldimethylsilyl)oxy]-2-methyl-1,3-cyclohexadiene

: 87598-75-2
benzyl 2-hydroxy-3-methyl-6-<3(S)-formylbutyl>benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 54 percent / pyrogallol / 12 h / Ambient temperature

2: 98 percent / cupric acetate monohydrate / diethyl ether / 1.) -35 to -25 deg C, 30 min, 2.) to room temp., 30 min

3: 97 percent / 12 h / 160 °C / sealed evacuated ampule

4: 94 percent / sodium metaperiodate / methanol; H₂O / 0.5 h / Ambient temperature

With sodium periodate; copper diacetate; 2-hydroxyresorcinol; In methanol; diethyl ether; water;
DOI:10.1021/jo00174a008

Reference yield:

: 87598-76-3
bromopropynoic acid benzyl ester

: 87598-75-2
benzyl 2-hydroxy-3-methyl-6-<3(S)-formylbutyl>benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 54 percent / pyrogallol / 12 h / Ambient temperature

2: 98 percent / cupric acetate monohydrate / diethyl ether / 1.) -35 to -25 deg C, 30 min, 2.) to room temp., 30 min

3: 97 percent / 12 h / 160 °C / sealed evacuated ampule

4: 94 percent / sodium metaperiodate / methanol; H₂O / 0.5 h / Ambient temperature

With sodium periodate; copper diacetate; 2-hydroxyresorcinol; In methanol; diethyl ether; water;
DOI:10.1021/jo00174a008

Reference yield:

: 87598-81-0
3-bromo-1-<(tert-butyldimethylsilyl)oxy>-2-(carbobenzyloxy)-6-methylbicyclo<2.2.2>octadiene

: 87598-75-2
benzyl 2-hydroxy-3-methyl-6-<3(S)-formylbutyl>benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / cupric acetate monohydrate / diethyl ether / 1.) -35 to -25 deg C, 30 min, 2.) to room temp., 30 min

2: 97 percent / 12 h / 160 °C / sealed evacuated ampule

3: 94 percent / sodium metaperiodate / methanol; H₂O / 0.5 h / Ambient temperature

With sodium periodate; copper diacetate; In methanol; diethyl ether; water;
DOI:10.1021/jo00174a008