Silane, [3-[9-[4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]butyl]-8-(phenylsulfonyl)-1,4- dioxaspiro[4.5]dec-6-en-8-yl]-1-methyl-1-propenyl]trimethyl-

Base Information

Chemical Name:Silane, [3-[9-[4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]butyl]-8-(phenylsulfonyl)-1,4- dioxaspiro[4.5]dec-6-en-8-yl]-1-methyl-1-propenyl]trimethyl-
CAS No.:87640-88-8
Molecular Formula:C₃₁H₅₂O₅SSi₂
Molecular Weight:592.988
Hs Code.:

Silane,
[3-[9-[4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]butyl]-8-(phenylsulfonyl)-1,4-
dioxaspiro[4.5]dec-6-en-8-yl]-1-methyl-1-propenyl]trimethyl-

Synonyms:

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Chemical Property of Silane, [3-[9-[4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]butyl]-8-(phenylsulfonyl)-1,4- dioxaspiro[4.5]dec-6-en-8-yl]-1-methyl-1-propenyl]trimethyl-

Chemical Property:

Purity/Quality:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Silane, [3-[9-[4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]butyl]-8-(phenylsulfonyl)-1,4- dioxaspiro[4.5]dec-6-en-8-yl]-1-methyl-1-propenyl]trimethyl-

There total 8 articles about Silane, [3-[9-[4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]butyl]-8-(phenylsulfonyl)-1,4- dioxaspiro[4.5]dec-6-en-8-yl]-1-methyl-1-propenyl]trimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 821-41-0
5-Hexen-1-ol

: 87640-88-8
8-Benzenesulfonyl-9-[4-(tert-butyl-dimethyl-silanyloxy)-butyl]-8-((E)-3-trimethylsilanyl-but-2-enyl)-1,4-dioxa-spiro[4.5]dec-6-ene

Guidance literature:: Multi-step reaction with 4 steps

1: 65 percent / imidazole / dimethylformamide / 20 h / Heating

2: 89 percent / CCl₄ / Irradiation

3: 2.) p-toluenesulfonic acid / 1.) xylene, reflux, 48 h, 2.) benzene, 20 h, reflux

4: 1.) NaH / 1.) DMF, 2.) 17.5 h

With 1H-imidazole; sodium hydride; toluene-4-sulfonic acid; In tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00173a040

Reference yield:

: 60805-71-2
phenylselenyl benzenesulfonate

: 87640-88-8
8-Benzenesulfonyl-9-[4-(tert-butyl-dimethyl-silanyloxy)-butyl]-8-((E)-3-trimethylsilanyl-but-2-enyl)-1,4-dioxa-spiro[4.5]dec-6-ene

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / CCl₄ / Irradiation

2: 2.) p-toluenesulfonic acid / 1.) xylene, reflux, 48 h, 2.) benzene, 20 h, reflux

3: 1.) NaH / 1.) DMF, 2.) 17.5 h

With sodium hydride; toluene-4-sulfonic acid; In tetrachloromethane;
DOI:10.1021/jo00173a040

Reference yield:

: 85807-84-7
tert-butyl(5-hexenyloxy)dimethylsilane

: 87640-88-8
8-Benzenesulfonyl-9-[4-(tert-butyl-dimethyl-silanyloxy)-butyl]-8-((E)-3-trimethylsilanyl-but-2-enyl)-1,4-dioxa-spiro[4.5]dec-6-ene

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / CCl₄ / Irradiation

2: 2.) p-toluenesulfonic acid / 1.) xylene, reflux, 48 h, 2.) benzene, 20 h, reflux

3: 1.) NaH / 1.) DMF, 2.) 17.5 h

With sodium hydride; toluene-4-sulfonic acid; In tetrachloromethane;
DOI:10.1021/jo00173a040