Benzoic acid, 3-bromo-4-methoxy-, 1,1-dimethylethyl ester

Base Information

Chemical Name:Benzoic acid, 3-bromo-4-methoxy-, 1,1-dimethylethyl ester
CAS No.:876752-69-1
Molecular Formula:C12H15BrO3
Molecular Weight:287.153
Hs Code.:

Synonyms:3-bromo-4-methoxybenzoic acid tert-butyl ester;Benzoic acid,3-bromo-4-methoxy-,1,1-dimethylethyl ester;

Suppliers and Price of Benzoic acid, 3-bromo-4-methoxy-, 1,1-dimethylethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of Benzoic acid, 3-bromo-4-methoxy-, 1,1-dimethylethyl ester

Chemical Property:

PSA：35.53000
LogP:3.41300

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzoic acid, 3-bromo-4-methoxy-, 1,1-dimethylethyl ester

There total 2 articles about Benzoic acid, 3-bromo-4-methoxy-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 99-58-1
3-bromo-4-methoxybenzoic acid

: 75-65-0
tert-butyl alcohol

: 876752-69-1
3-bromo-4-methoxybenzoic acid tert-butyl ester

Guidance literature:: With dmap; di-tert-butyl dicarbonate; for 10h; Heating;
DOI:10.1021/ol0623926

Reference yield: 24.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 99-58-1
3-bromo-4-methoxybenzoic acid

: 876752-69-1
3-bromo-4-methoxybenzoic acid tert-butyl ester

Guidance literature:: With dmap; In tert-butyl alcohol; at 50 ℃; Inert atmosphere;

Reference yield: 85.0%

: 876752-69-1
3-bromo-4-methoxybenzoic acid tert-butyl ester

: tert-butyl 1-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-6-azaspiro[2.5]octane-6-carboxylate

: C₃₀H₃₉NO₅

Guidance literature:: With potassium phosphate; bis(di-tert-butyl(4-dimethylaminophenyl)phosphine)dichloropalladium(II); In 1,4-dioxane; water; at 80 ℃; for 2h; Inert atmosphere;