(1,1-Diphenylprop-1-en-2-yl)(trimethyl)silane

Base Information

• Chemical Name: (1,1-Diphenylprop-1-en-2-yl)(trimethyl)silane
• CAS No.: 87729-76-8
• Molecular Formula: C₁₈H₂₂Si
• Molecular Weight: 266.458
• DSSTox Substance ID: DTXSID40520353

Synonyms:(1,1-Diphenylprop-1-en-2-yl)(trimethyl)silane;87729-76-8;DTXSID40520353

Chemical Property of (1,1-Diphenylprop-1-en-2-yl)(trimethyl)silane

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 3
• Exact Mass: 266.149077236
• Heavy Atom Count: 19
• Complexity: 289

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=C(C1=CC=CC=C1)C2=CC=CC=C2)[Si](C)(C)C

Technology Process of (1,1-Diphenylprop-1-en-2-yl)(trimethyl)silane

There total 2 articles about (1,1-Diphenylprop-1-en-2-yl)(trimethyl)silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzophenone (119-61-9) + 1,1-Bis(trimethylsilyl)-1-(phenylthio)ethane (87739-09-1) → Trimethyl-(1-methyl-2,2-diphenyl-vinyl)-silane (87729-76-8)

Guidance literature:

With lithium 1-naphthalenide; Yield given. Multistep reaction; 1) THF, 4 h, -78 deg C; 2) r.t.;

DOI:10.1021/jo00175a036

Reference yield:

(Z)-2-methyl-1-phenyl-2-(trimethylsilyl)vinyl diphenyl phosphate (118297-87-3) + phenylmagnesium bromide → Trimethyl-(1-methyl-2,2-diphenyl-vinyl)-silane (87729-76-8)

Guidance literature:

With 1.) CuCN; Yield given. Multistep reaction; 1.) THF, ether, 0 deg C, 15 min, 2.) 2 h;

DOI:10.1021/jo00265a005

upstream raw materials:

benzophenone

1,1-Bis(trimethylsilyl)-1-(phenylthio)ethane

(Z)-2-methyl-1-phenyl-2-(trimethylsilyl)vinyl diphenyl phosphate

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