[1,1-Bis(phenylsulfanyl)ethyl](trimethyl)silane

Base Information

Chemical Name:[1,1-Bis(phenylsulfanyl)ethyl](trimethyl)silane
CAS No.:87729-81-5
Molecular Formula:C₁₇H₂₂S₂Si
Molecular Weight:318.579
Hs Code.:
DSSTox Substance ID:DTXSID60520350
Wikidata:Q82384192

Synonyms:[1,1-Bis(phenylsulfanyl)ethyl](trimethyl)silane;87729-81-5;DTXSID60520350

Suppliers and Price of [1,1-Bis(phenylsulfanyl)ethyl](trimethyl)silane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [1,1-Bis(phenylsulfanyl)ethyl](trimethyl)silane

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:318.09321958
Heavy Atom Count:20
Complexity:266

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC([Si](C)(C)C)(SC1=CC=CC=C1)SC2=CC=CC=C2

Technology Process of [1,1-Bis(phenylsulfanyl)ethyl](trimethyl)silane

There total 1 articles about [1,1-Bis(phenylsulfanyl)ethyl](trimethyl)silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 37891-39-7
trimethylsilane

: 74-88-4
methyl iodide

: 87729-81-5
1,1-Bis(phenylthio)-1-(trimethylsilyl)ethane

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1.) THF, 0 deg C, 1 h; 2.) 1 h;
DOI:10.1021/jo00175a036

Reference yield:

: 87729-81-5
1,1-Bis(phenylthio)-1-(trimethylsilyl)ethane

: (1-Benzenesulfinyl-1-methyl-pentyl)-trimethyl-silane

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) lithium naphthalenide / 1.) 2 h, 2.) TMEDA, room temperature

2: 85percent m-chloroperbenzoic acid / CH₂Cl₂ / 1.5 h / -23 °C

With naphthalen-1-yl-lithium; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1039/P19860000195

Reference yield:

: 87729-81-5
1,1-Bis(phenylthio)-1-(trimethylsilyl)ethane

: (1-Benzenesulfinyl-1-methyl-ethyl)-trimethyl-silane

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) lithium naphthalenide / 1.) 2 h, 2.) TMEDA, room temperature

2: 85percent m-chloroperbenzoic acid / CH₂Cl₂ / 1.5 h / -23 °C

With naphthalen-1-yl-lithium; 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1039/P19860000195