Technology Process of Carbamic acid,
[3-(2,3-dimethoxyphenyl)-3-(1,3-dithian-2-yl)propyl](hydroxymethyl)-,
ethyl ester
There total 7 articles about Carbamic acid,
[3-(2,3-dimethoxyphenyl)-3-(1,3-dithian-2-yl)propyl](hydroxymethyl)-,
ethyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydroxide;
In
methanol;
for 12h;
Ambient temperature;
DOI:10.1021/jo00175a033
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 96 percent / benzyltrimethylammonium hydroxide / acetonitrile / 24 h / Heating
2: 90 percent / conc.H2SO4 / methanol / 0.33 h / -35 °C
3: 45 percent / boron trifluoride etherate / Ambient temperature
4: 99 percent / lithium aluminium hydride, AlCl3 / tetrahydrofuran / 1.5 h / 40 °C
5: 100 percent / triethylamine / CH2Cl2 / 0.5 h
6: 100 percent / 25percent aq.NaOH / methanol / 12 h / Ambient temperature
With
sodium hydroxide; lithium aluminium tetrahydride; aluminium trichloride; sulfuric acid; boron trifluoride diethyl etherate; N-benzyl-trimethylammonium hydroxide; triethylamine;
In
tetrahydrofuran; methanol; dichloromethane; acetonitrile;
DOI:10.1021/jo00175a033
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 90 percent / conc.H2SO4 / methanol / 0.33 h / -35 °C
2: 45 percent / boron trifluoride etherate / Ambient temperature
3: 99 percent / lithium aluminium hydride, AlCl3 / tetrahydrofuran / 1.5 h / 40 °C
4: 100 percent / triethylamine / CH2Cl2 / 0.5 h
5: 100 percent / 25percent aq.NaOH / methanol / 12 h / Ambient temperature
With
sodium hydroxide; lithium aluminium tetrahydride; aluminium trichloride; sulfuric acid; boron trifluoride diethyl etherate; triethylamine;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jo00175a033
