N-(Acetyloxy)-N-[(cyclohex-1-en-1-yl)methyl]pent-4-enamide

Base Information

Chemical Name:N-(Acetyloxy)-N-[(cyclohex-1-en-1-yl)methyl]pent-4-enamide
CAS No.:87842-77-1
Molecular Formula:C14H21NO3
Molecular Weight:251.326
Hs Code.:
DSSTox Substance ID:DTXSID10520264
Wikidata:Q82384055

Synonyms:87842-77-1;DTXSID10520264;N-(Acetyloxy)-N-[(cyclohex-1-en-1-yl)methyl]pent-4-enamide

Suppliers and Price of N-(Acetyloxy)-N-[(cyclohex-1-en-1-yl)methyl]pent-4-enamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of N-(Acetyloxy)-N-[(cyclohex-1-en-1-yl)methyl]pent-4-enamide

Chemical Property:

XLogP3:2.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:7
Exact Mass:251.15214353
Heavy Atom Count:18
Complexity:347

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)ON(CC1=CCCCC1)C(=O)CCC=C

Technology Process of N-(Acetyloxy)-N-[(cyclohex-1-en-1-yl)methyl]pent-4-enamide

There total 3 articles about N-(Acetyloxy)-N-[(cyclohex-1-en-1-yl)methyl]pent-4-enamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 39716-58-0
pent-4-enoyl chloride

: 87842-90-8
O-acetyl-N-(cyclohexenylmethyl)hydroxylamine

: 87842-77-1
O-acetyl-N-(cyclohexenylmethyl)-N-4-pentenoylhydroxylamine

Guidance literature:: With triethylamine; In tetrachloromethane; for 1h; Ambient temperature;
DOI:10.1021/ja00364a040

Reference yield:

: 37677-17-1
1-bromomethylcyclohexene

: 87842-77-1
O-acetyl-N-(cyclohexenylmethyl)-N-4-pentenoylhydroxylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / K₂CO₃ / dimethylformamide / 20 h / Ambient temperature

2: 40 percent / 6N HCl / 1 h / Ambient temperature

3: 74 percent / Et₃N / CCl₄ / 1 h / Ambient temperature

With hydrogenchloride; potassium carbonate; triethylamine; In tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja00364a040

Reference yield:

: 87842-89-5
N,O-diacetyl-N-(cyclohexenylmethyl)hydroxylamine

: 87842-77-1
O-acetyl-N-(cyclohexenylmethyl)-N-4-pentenoylhydroxylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 40 percent / 6N HCl / 1 h / Ambient temperature

2: 74 percent / Et₃N / CCl₄ / 1 h / Ambient temperature

With hydrogenchloride; triethylamine; In tetrachloromethane;
DOI:10.1021/ja00364a040