5-Benzyl-5,6-dihydrophenanthridine

Base Information

Chemical Name:5-Benzyl-5,6-dihydrophenanthridine
CAS No.:87861-94-7
Molecular Formula:C20H17N
Molecular Weight:271.362
Hs Code.:
DSSTox Substance ID:DTXSID40518013
Nikkaji Number:J329.400E
Wikidata:Q82380374

Synonyms:5-BENZYL-5,6-DIHYDROPHENANTHRIDINE;87861-94-7;SCHEMBL18176034;DTXSID40518013

Suppliers and Price of 5-Benzyl-5,6-dihydrophenanthridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 5-Benzyl-5,6-dihydrophenanthridine

Chemical Property:

XLogP3:4.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:271.136099547
Heavy Atom Count:21
Complexity:333

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C2=CC=CC=C2C3=CC=CC=C3N1CC4=CC=CC=C4

Technology Process of 5-Benzyl-5,6-dihydrophenanthridine

There total 13 articles about 5-Benzyl-5,6-dihydrophenanthridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1075193-04-2
N,N-dibenzyl-2-bromoaniline

: 87861-94-7
5-benzyl-5,6-dihydrophenanthridine

Guidance literature:: With 2.9-dimethyl-1,10-phenanthroline; potassium tert-butylate; In benzene; at 100 ℃; for 24h; Inert atmosphere;
DOI:10.1039/c1cc13907j

Reference yield: 65.0%

: 1308865-49-7
N,N-dibenzyl-2-iodoaniline

: 87861-94-7
5-benzyl-5,6-dihydrophenanthridine

Guidance literature:: With pyridine; potassium tert-butylate; at 20 - 160 ℃; for 0.183333h; regioselective reaction; Inert atmosphere; Microwave irradiation;
DOI:10.1021/ol201160s

Reference yield:

: 229-87-8
phenanthridine

: 87861-94-7
5-benzyl-5,6-dihydrophenanthridine

Guidance literature:: Multi-step reaction with 2 steps

1: ethanol

2: NaBH₄

With sodium tetrahydroborate; In ethanol;
DOI:10.1021/ja00364a026