INDAN-2 2-DICARBOXYLIC ACID 97

Base Information

• Chemical Name: INDAN-2 2-DICARBOXYLIC ACID 97
• CAS No.: 2437-08-3
• Molecular Formula: C11H10 O4
• Molecular Weight: 206.198
• Hs Code.: 2917399090
• Mol file: 2437-08-3.mol

Synonyms:2,2-Indandicarboxylicacid; 2,2-Indanedicarboxylic acid; NSC 73040

Chemical Property of INDAN-2 2-DICARBOXYLIC ACID 97

Chemical Property:

• Vapor Pressure: 3.87E-09mmHg at 25°C
• Melting Point: 191-195 °C (dec.)(lit.)
• Boiling Point: 456.8°Cat760mmHg
• Flash Point: 244.2°C
• PSA: 74.60000
• Density: 1.457g/cm³
• LogP: 0.94080

Purity/Quality:

98%,99%, ^*data from raw suppliers

1,3-Dihydroindene-2,2-dicarboxylicacid ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of INDAN-2 2-DICARBOXYLIC ACID 97

There total 7 articles about INDAN-2 2-DICARBOXYLIC ACID 97 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

diethyl indan-2,2-dicarboxylate (66014-45-7) → indane-2,2-dicarboxylic acid (2437-08-3)

Guidance literature:

With potassium hydroxide; In ethanol; for 12h; Heating;

DOI:10.1002/hlca.19940770729

Reference yield:

α,α-dibromo-o-xylene (79985-01-6) + diethyl malonate (105-53-3) → indane-2,2-dicarboxylic acid (2437-08-3)

Guidance literature:

With potassium hydroxide; sodium; In diethyl ether; ethanol; water;

Reference yield:

α,α'-dibromo-o-xylene (91-13-4) + diethyl malonate (105-53-3) → indane-2,2-dicarboxylic acid (2437-08-3)

Guidance literature:

With potassium hydroxide; sodium; In diethyl ether; ethanol; water;

upstream raw materials:

diethyl indan-2,2-dicarboxylate

sodium diethylmalonate

α,α'-dibromo-o-xylene

α,α-dibromo-o-xylene

Downstream raw materials:

INDANE

2,2-bis((4R,5S)-4,5-diphenyl-4,5-dihydrooxazol-2-yl)-2,3-dihydro-1H-inden

5-nitroindane-2-carboxylic acid

(2-indan-2-yl-2-oxoethyl)phosphonic acid dimethyl ester

Refernces

• 1、 Bergmann,Hoffmann. "". . p. 3555. Retrieved 1961.
• 2、 Barman, Samir,Khutia, Anupam,Koitz, Ralph,Blacque, Olivier,Furukawa, Hiroyasu,Iannuzzi, Marcella,Yaghi, Omar M.,Janiak, Christoph,Hutter, Jürg,Berke, Heinz. "Synthesis and hydrogen adsorption properties of internally polarized 2,6-azulenedicarboxylate based metal-organic frameworks". supporting information. p. 18823 - 18830. Retrieved 2014/12/11.
• 3、 -. "Mercaptocycloacyl aminoacid endopeptidase inhibitors". . . Retrieved 2008/06/13.