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Samarium, iodophenyl-

Base Information
  • Chemical Name:Samarium, iodophenyl-
  • CAS No.:88020-61-5
  • Molecular Formula:C6H5ISm
  • Molecular Weight:354.37
  • Hs Code.:
Samarium, iodophenyl-

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Chemical Property of Samarium, iodophenyl-
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Technology Process of Samarium, iodophenyl-

There total 1 articles about Samarium, iodophenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In tetrahydrofuran; Ar atmosphere; alkylation of metal with CH2I2 in THF, then reaction with PhI; not isolated;
DOI:10.1007/BF00957447
Guidance literature:
In tetrahydrofuran; at -40 ℃; for 0.666667h;
DOI:10.1007/BF00954722
Guidance literature:
With water; In tetrahydrofuran; byproducts: trimethylhydroxosilane, hexamethyldisiloxane; under Ar; addn. of freshly prepd. THF soln. of PhSmI to mixt. of THF and Ph3SnSiMe3, mixing at 25°C for 3 h, decompn. of react. mixt. with water acidified with HCl; thin layer chromy.;
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