Technology Process of Samarium
There total 25 articles about Samarium which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
zirconium;
In
neat (no solvent);
reduction by heating the pressesd mixture (99.05 Sm2O3, purity of reducing reagent >99.5%) to 1100-1200°C at maximal 2E-4 Torr, distn. of Sm, Mo-vessel;;;
- Guidance literature:
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vapor pressure of Sm between 1217 and 1473°K given as equation; optimal conditions: 1200°C, 1E-3 Torr;
- Guidance literature:
-
In
ethylenediamine;
Electrolysis; 150V, 4.4mA/cm**2, 0.37g nitrate in ethylene diamine;;