(8-chloro-3,5-dihydro-2H-furo[2,3-f]indol-2-yl)methyl acetate

Base Information

Chemical Name:(8-chloro-3,5-dihydro-2H-furo[2,3-f]indol-2-yl)methyl acetate
CAS No.:88062-21-9
Molecular Formula:C₁₃H₁₂ClNO₃
Molecular Weight:265.696
Hs Code.:

Synonyms:

Suppliers and Price of (8-chloro-3,5-dihydro-2H-furo[2,3-f]indol-2-yl)methyl acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 2 raw suppliers

Chemical Property of (8-chloro-3,5-dihydro-2H-furo[2,3-f]indol-2-yl)methyl acetate

Chemical Property:

Vapor Pressure:9.58E-08mmHg at 25°C

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (8-chloro-3,5-dihydro-2H-furo[2,3-f]indol-2-yl)methyl acetate

There total 5 articles about (8-chloro-3,5-dihydro-2H-furo[2,3-f]indol-2-yl)methyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 88062-19-5
2-(acetoxymethyl)-7-chloro-2,3-dihydro-5-nitro-6-(β-nitrovinyl)benzofuran

: 88062-21-9
2-(acetoxymethyl)-8-chloro-3,5-dihydro-2H-furo<2,3-f>indole

Guidance literature:: With iron; In ethanol; acetic acid; for 0.416667h;
DOI:10.1002/jhet.5570200443

Reference yield:

: 19183-03-0
2-chloro-6-nitro-3-hydroxybenzaldehyde

: 88062-21-9
2-(acetoxymethyl)-8-chloro-3,5-dihydro-2H-furo<2,3-f>indole

Guidance literature:: Multi-step reaction with 5 steps

1: 87 percent / K₂CO₃ / dimethylformamide / 6 h / 60 °C

2: 47 percent / diphenyl ether / 1 h / 225 - 230 °C

3: 64 percent / 85percent m-chloroperoxybenzoic acid / CH₂Cl₂ / 20 h / Ambient temperature

4: 1) NaOH; 2) CH₃COONa / 1) methanol, water, THF, 10 deg C, 1 h; 2) 140 deg C, 30 min.

5: 85 percent / Fe powder / ethanol; acetic acid / 0.42 h

With sodium hydroxide; sodium acetate; iron; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In diphenylether; ethanol; dichloromethane; acetic acid; N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570200443

Reference yield:

: 344559-44-0
3-Allyloxy-2-chloro-6-nitro-benzaldehyde

: 88062-21-9
2-(acetoxymethyl)-8-chloro-3,5-dihydro-2H-furo<2,3-f>indole

Guidance literature:: Multi-step reaction with 4 steps

1: 47 percent / diphenyl ether / 1 h / 225 - 230 °C

2: 64 percent / 85percent m-chloroperoxybenzoic acid / CH₂Cl₂ / 20 h / Ambient temperature

3: 1) NaOH; 2) CH₃COONa / 1) methanol, water, THF, 10 deg C, 1 h; 2) 140 deg C, 30 min.

4: 85 percent / Fe powder / ethanol; acetic acid / 0.42 h

With sodium hydroxide; sodium acetate; iron; 3-chloro-benzenecarboperoxoic acid; In diphenylether; ethanol; dichloromethane; acetic acid;
DOI:10.1002/jhet.5570200443