Sulfoxylic diamide, tetrakis(phenylmethyl)-

Base Information

Chemical Name:Sulfoxylic diamide, tetrakis(phenylmethyl)-
CAS No.:88072-44-0
Molecular Formula:C28H28N2S
Molecular Weight:424.61
Hs Code.:

Synonyms:bis-dibenzylamino-sulfane;Bis-dibenzylamino-sulfan;Bis-dibenzylamino-sulfid;thiobisdibenzylamine;2,4-dibenzyl-1,5-diphenyl-2,4-diaza-3-thiapentane;N,N'-thiobisdibenzylamine;

Suppliers and Price of Sulfoxylic diamide, tetrakis(phenylmethyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Sulfoxylic diamide, tetrakis(phenylmethyl)-

Chemical Property:

Boiling Point:587.9±60.0 °C(Predicted)
PSA：31.78000
Density:1.160±0.06 g/cm3(Predicted)
LogP:6.95440

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Sulfoxylic diamide, tetrakis(phenylmethyl)-

There total 1 articles about Sulfoxylic diamide, tetrakis(phenylmethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 103-49-1
dibenzylamine

: 88072-44-0
2,4-dibenzyl-1,5-diphenyl-2,4-diaza-3-thiapentane

Guidance literature:: With sulfur dichloride;

Reference yield: 30.0%

: 88072-44-0
2,4-dibenzyl-1,5-diphenyl-2,4-diaza-3-thiapentane

: 199620-14-9,13007-92-6
chromium⁽⁰⁾ hexacarbonyl

: 91217-36-6
Cr(CO)5S(N(CH₂C₆H₅)2)2

Guidance literature:: In tetrahydrofuran; Irradiation (UV/VIS); soln. Cr(CO)6 in THF irradiated (UV Lamp Hanovia, medium pressure 150 w) for 90 min at room temp., soln. thiobisamine in THF added and mixt. stirred for 60 min; solvent removed under reduced pressure, excess hexacarbonyl sublimed under vac. at room temp., solid redissolved in n-hexane-n-pentane mixt., filtered, solvent evapd.; elem. anal.;
DOI:10.1016/S0020-1693(00)81027-0

Reference yield:

: copper(II) choride dihydrate

: 88072-44-0
2,4-dibenzyl-1,5-diphenyl-2,4-diaza-3-thiapentane

: N,N-dibenzylammonium trichlorodicuprate(I)

: 20455-68-9
N,N-dibenzylamine hydrochloride

Guidance literature:: In ethanol; byproducts: SO2; addn. of S(N(CH2C6H5)2)2 soln. to soln. of CuCl2*2H2O in ethanol previously deoxygenated with nitrogen, reaction under oxygen free nitrogen; stirring at room temp.;; product mixt. in soln. obtained; pptn. of mixt. by addn. of cyclohexane; filtration; drying in vac.; white solid was isolated whose elem. anal. suggested a mixture of 65% ((C6H5CH2)2NH2)(Cu2Cl3) and 35% ((C6H5CH2(2NH2)Cl; IR spectroscopy;;
DOI:10.1016/S0277-5387(00)84414-9