1-(9H-Fluoren-2-yl)-2-(triphenyl-lambda~5~-phosphanylidene)ethan-1-one

Base Information

Chemical Name:1-(9H-Fluoren-2-yl)-2-(triphenyl-lambda~5~-phosphanylidene)ethan-1-one
CAS No.:88092-98-2
Molecular Formula:C₃₃H₂₅OP
Molecular Weight:468.535
Hs Code.:
DSSTox Substance ID:DTXSID20520932
Wikidata:Q82385111

Synonyms:88092-98-2;1-(9H-Fluoren-2-yl)-2-(triphenylphosphoranylidene)ethanone;DTXSID20520932;1-(9H-Fluoren-2-yl)-2-(triphenyl-lambda~5~-phosphanylidene)ethan-1-one

Suppliers and Price of 1-(9H-Fluoren-2-yl)-2-(triphenyl-lambda~5~-phosphanylidene)ethan-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 1-(9H-Fluoren-2-yl)-2-(triphenyl-lambda~5~-phosphanylidene)ethan-1-one

Chemical Property:

XLogP3:6.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:5
Exact Mass:468.164302414
Heavy Atom Count:35
Complexity:714

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C2=CC=CC=C2C3=C1C=C(C=C3)C(=O)C=P(C4=CC=CC=C4)(C5=CC=CC=C5)C6=CC=CC=C6

Technology Process of 1-(9H-Fluoren-2-yl)-2-(triphenyl-lambda~5~-phosphanylidene)ethan-1-one

There total 2 articles about 1-(9H-Fluoren-2-yl)-2-(triphenyl-lambda~5~-phosphanylidene)ethan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 781-73-7
1-(9H-fluoren-2-yl)ethanone

: 88092-98-2,88093-11-2
1-(9H-Fluoren-2-yl)-2-(triphenyl-λ⁵-phosphanylidene)-ethanone

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / Br₂ / diethyl ether; dioxane / 0.5 h

2: 92 percent / benzene / 20 h / Heating

3: 68 percent / NaOEt / ethanol / 0.5 h

With bromine; sodium ethanolate; In 1,4-dioxane; diethyl ether; ethanol; benzene;

Reference yield:

: 39696-13-4
2-bromo-1-(9H-fluoren-2-yl)ethanone

: 88092-98-2,88093-11-2
1-(9H-Fluoren-2-yl)-2-(triphenyl-λ⁵-phosphanylidene)-ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / benzene / 20 h / Heating

2: 68 percent / NaOEt / ethanol / 0.5 h

With sodium ethanolate; In ethanol; benzene;