Benzamide, N-(2-formylphenyl)-2-nitro-

Base Information

Chemical Name:Benzamide, N-(2-formylphenyl)-2-nitro-
CAS No.:88116-43-2
Molecular Formula:C14H10N2O4
Molecular Weight:270.244
Hs Code.:
DSSTox Substance ID:DTXSID60457016
Wikidata:Q82279684

Synonyms:Benzamide, N-(2-formylphenyl)-2-nitro-;88116-43-2;DTXSID60457016

Suppliers and Price of Benzamide, N-(2-formylphenyl)-2-nitro-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzamide, N-(2-formylphenyl)-2-nitro-

Chemical Property:

XLogP3:2.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:270.06405680
Heavy Atom Count:20
Complexity:380

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C(=C1)C=O)NC(=O)C2=CC=CC=C2[N+](=O)[O-]

Technology Process of Benzamide, N-(2-formylphenyl)-2-nitro-

There total 3 articles about Benzamide, N-(2-formylphenyl)-2-nitro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 529-23-7
o-aminobenzaldehyde

: 610-14-0
2-nitrobenzyl chloride

: 88116-43-2
N-(2'-formylphenyl)-2-nitrobenzamide

Guidance literature:: With triethylamine; In dichloromethane; Cooling with ice;
DOI:10.1002/ejoc.201501359

Reference yield:

: 552-16-9,104810-18-6
ortho-nitrobenzoic acid

: 88116-43-2
N-(2'-formylphenyl)-2-nitrobenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 3 h / 50 °C

2: 91 percent / pyridine / tetrahydrofuran / 8 h / 20 °C

3: 86 percent / pyridinium chlorochromate / CH₂Cl₂ / 25 °C

With pyridine; thionyl chloride; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane;
DOI:10.1081/SCC-200057990

Reference yield:

: 610-14-0
2-nitrobenzyl chloride

: 88116-43-2
N-(2'-formylphenyl)-2-nitrobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / pyridine / tetrahydrofuran / 8 h / 20 °C

2: 86 percent / pyridinium chlorochromate / CH₂Cl₂ / 25 °C

With pyridine; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane;
DOI:10.1081/SCC-200057990