Piperidine, 2-benzoyl-1-(2,2-diethyl-1-oxobutyl)-4-phenyl-, trans-

Base Information

Chemical Name:Piperidine, 2-benzoyl-1-(2,2-diethyl-1-oxobutyl)-4-phenyl-, trans-
CAS No.:88131-94-6
Molecular Formula:C26H33NO2
Molecular Weight:391.554
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Piperidine, 2-benzoyl-1-(2,2-diethyl-1-oxobutyl)-4-phenyl-, trans-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
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MSDS Files:: SDS file from LookChem

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Technology Process of Piperidine, 2-benzoyl-1-(2,2-diethyl-1-oxobutyl)-4-phenyl-, trans-

There total 7 articles about Piperidine, 2-benzoyl-1-(2,2-diethyl-1-oxobutyl)-4-phenyl-, trans- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 88131-93-5
2(e)-benzoyl-4-phenyl-2,2-diethylbutanopiperidide

: 88131-94-6
2(a)-benzoyl-4-phenyl-2,2-diethylbutanopiperidide

Guidance literature:: With sodium methylate; In methanol; for 2h; Heating;
DOI:10.1021/ja00316a033

Reference yield:

: 813-58-1
triethylacetic acid

: 88131-94-6
2(a)-benzoyl-4-phenyl-2,2-diethylbutanopiperidide

Guidance literature:: Multi-step reaction with 5 steps

1: thionyl chloride

2: 99 percent / sodium carbonate / H₂O; diethyl ether / 4 h

3: 1.) TMEDA, sec-BuLi / 1.) ether, 0 deg C, 1 h; 2.) -78 deg C -> ambient temp.

4: 90 percent / sodium acetate, pyridinium chlorochromate / CH₂Cl₂ / 2 h

5: 81 percent / sodium methoxide / methanol / 2 h / Heating

With thionyl chloride; N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; sodium methylate; sodium acetate; sodium carbonate; pyridinium chlorochromate; In methanol; diethyl ether; dichloromethane; water;
DOI:10.1021/ja00316a033

Reference yield:

: 35354-15-5
2,2-diethylbutanoyl chloride

: 88131-94-6
2(a)-benzoyl-4-phenyl-2,2-diethylbutanopiperidide

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / sodium carbonate / H₂O; diethyl ether / 4 h

2: 1.) TMEDA, sec-BuLi / 1.) ether, 0 deg C, 1 h; 2.) -78 deg C -> ambient temp.

3: 90 percent / sodium acetate, pyridinium chlorochromate / CH₂Cl₂ / 2 h

4: 81 percent / sodium methoxide / methanol / 2 h / Heating

With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; sodium methylate; sodium acetate; sodium carbonate; pyridinium chlorochromate; In methanol; diethyl ether; dichloromethane; water;
DOI:10.1021/ja00316a033