N-(3-Chlorophenyl)-N-(2,2-diethoxyethyl)methanesulfonamide

Base Information

Chemical Name:N-(3-Chlorophenyl)-N-(2,2-diethoxyethyl)methanesulfonamide
CAS No.:88156-70-1
Molecular Formula:C13H20ClNO4S
Molecular Weight:321.825
Hs Code.:
DSSTox Substance ID:DTXSID00530195
Wikidata:Q82401179

Synonyms:88156-70-1;DTXSID00530195;N-(3-Chlorophenyl)-N-(2,2-diethoxyethyl)methanesulfonamide

Suppliers and Price of N-(3-Chlorophenyl)-N-(2,2-diethoxyethyl)methanesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of N-(3-Chlorophenyl)-N-(2,2-diethoxyethyl)methanesulfonamide

Chemical Property:

XLogP3:2.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:8
Exact Mass:321.0801570
Heavy Atom Count:20
Complexity:365

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(CN(C1=CC(=CC=C1)Cl)S(=O)(=O)C)OCC

Technology Process of N-(3-Chlorophenyl)-N-(2,2-diethoxyethyl)methanesulfonamide

There total 2 articles about N-(3-Chlorophenyl)-N-(2,2-diethoxyethyl)methanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 7022-21-1
N-(3-chlorophenyl)methanesulfonamide

: 2032-35-1
Bromoacetaldehyde diethyl acetal

: 88156-70-1
N-(3-Chloro-phenyl)-N-(2,2-diethoxy-ethyl)-methanesulfonamide

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 110 ℃;
DOI:10.1021/jo00176a007

Reference yield:

: 108-42-9
3-chloro-aniline

: 88156-70-1
N-(3-Chloro-phenyl)-N-(2,2-diethoxy-ethyl)-methanesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / CH₂Cl₂ / 1) 1 h, 0 deg C; 2) 1 h, 25 deg C

2: 62 percent / NaH / dimethylformamide / 110 °C

With pyridine; sodium hydride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00176a007

Reference yield:

: 88156-70-1
N-(3-Chloro-phenyl)-N-(2,2-diethoxy-ethyl)-methanesulfonamide

: 17422-33-2
6-chloroindole

Guidance literature:: Multi-step reaction with 2 steps

1: TiCl₄ / toluene / 110 °C

2: 90 percent / KOH / methanol / 18 h / Heating

With potassium hydroxide; titanium tetrachloride; In methanol; toluene;
DOI:10.1021/jo00176a007