1,4-Dioxaspiro[4.5]decan-8-one, 7-(3,4-dimethoxyphenyl)-

Base Information

Chemical Name:1,4-Dioxaspiro[4.5]decan-8-one, 7-(3,4-dimethoxyphenyl)-
CAS No.:88176-84-5
Molecular Formula:C16H20O5
Molecular Weight:292.332
Hs Code.:

Synonyms:

Suppliers and Price of 1,4-Dioxaspiro[4.5]decan-8-one, 7-(3,4-dimethoxyphenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of 1,4-Dioxaspiro[4.5]decan-8-one, 7-(3,4-dimethoxyphenyl)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,4-Dioxaspiro[4.5]decan-8-one, 7-(3,4-dimethoxyphenyl)-

There total 6 articles about 1,4-Dioxaspiro[4.5]decan-8-one, 7-(3,4-dimethoxyphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 88176-83-4
3-(3,4-dimethoxyphenyl)-3-cyclohexenone ethylene acetal

: 88176-84-5
3-(3,4-dimethoxyphenyl)-1,4-cyclohexanedione-1-(ethylene acetal)

Guidance literature:: Yield given. Multistep reaction;
DOI:10.1016/S0040-4039(00)86218-8

Reference yield:

: 5323-87-5
3-Ethoxycyclohex-2-en-1-one

: 88176-84-5
3-(3,4-dimethoxyphenyl)-1,4-cyclohexanedione-1-(ethylene acetal)

Guidance literature:: Multi-step reaction with 4 steps

1: 1) n-BuLi, 2) glacial acetic acid, 10percent aq. HCl / 1a) ether/hexane, -60 deg C, 1 h, 1b) RT, overnight

2: pyridinium p-toluenesulfonate / benzene / 120 h / Heating

3: 1) B₂H₆, 2) 3N NaOH, 30 percent H₂O₂ / 1) THF, RT, overnight, 2a) 45 deg C, 5 h, 2b) RT

4: sodium acetate, pyridinium chlorochromate / CH₂Cl₂

With hydrogenchloride; sodium hydroxide; n-butyllithium; dihydrogen peroxide; sodium acetate; pyridinium p-toluenesulfonate; acetic acid; pyridinium chlorochromate; diborane; In dichloromethane; benzene;
DOI:10.1021/jo00194a026