Phtiobuzone

Base Information

Chemical Name:Phtiobuzone
CAS No.:70386-40-2
Molecular Formula:C₁₄H₁₅N₇O₂S₂
Molecular Weight:377.451
Hs Code.:
UNII:S1199Y391N

Synonyms:2,2'-(1-(1-(1,3(2H)-dioxo-1H-isoindol-2-yl)ethyl)-1,2-ethanediylidene)bis-hydrazine carbothiamide;3-phthalimido-2-oxobutyraldehyde-bis-thiosemicarbazone;phthiobuzone;phtiobuzone;tai-ding-an;V-6133

Suppliers and Price of Phtiobuzone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of Phtiobuzone

Chemical Property:

Boiling Point:581.4°Cat760mmHg
Flash Point:305.4°C
Density:1.6g/cm³
XLogP3:0.3
Hydrogen Bond Donor Count:4
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:5
Exact Mass:377.07286509
Heavy Atom Count:25
Complexity:625

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C(=NNC(=S)N)C=NNC(=S)N)N1C(=O)C2=CC=CC=C2C1=O

Technology Process of Phtiobuzone

There total 5 articles about Phtiobuzone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 3-phthalimido-2-oxo-n-butyraldehyde

: 79-19-6
thiosemicarbazide

: 70386-40-2,79512-50-8
ftibamzone

Guidance literature:: In water; dimethyl sulfoxide; at 90 ℃; for 3h; Temperature;

Reference yield:

: 2-(2-hydroxy-1-methyl-propyl)-isoindole-1,3-dione

: 70386-40-2,79512-50-8
ftibamzone

Guidance literature:: Multi-step reaction with 3 steps

1: [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; 2,6-Di-tert-butyl-1,4-benzoquinone; manganese(IV) oxide / acetone / 17 h / 65 °C / Inert atmosphere

2: selenium(IV) oxide / 1,4-dioxane / 18 h / Reflux

3: ethanol; water / 1 h / Reflux

With manganese(IV) oxide; selenium(IV) oxide; [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; 2,6-Di-tert-butyl-1,4-benzoquinone; In 1,4-dioxane; ethanol; water; acetone;

Reference yield:

: 21860-84-4
2-phthalimidopropionic acid

: 70386-40-2,79512-50-8
ftibamzone

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran; diethyl ether / 1 h / -70 - 20 °C

2: selenium(IV) oxide / water; 1,4-dioxane / 20 h / 90 - 100 °C

3: water; ethanol / 2 h / 90 - 100 °C

With selenium(IV) oxide; In tetrahydrofuran; 1,4-dioxane; diethyl ether; ethanol; water;