4-(6-Hydroxyhexyloxy)-4'-cyanoazobenzene

Base Information

Chemical Name:4-(6-Hydroxyhexyloxy)-4'-cyanoazobenzene
CAS No.:88216-53-9
Molecular Formula:C19H21N3O2
Molecular Weight:323.38900
Hs Code.:
DSSTox Substance ID:DTXSID30598763
Nikkaji Number:J2.616.837F

Synonyms:4-(6-Hydroxyhexyloxy)-4'-cyanoazobenzene;88216-53-9;SCHEMBL7561155;SCHEMBL9004231;DTXSID30598763;NNLRLUPUDKZUSR-UHFFFAOYSA-N;4-[(E)-{4-[(6-Hydroxyhexyl)oxy]phenyl}diazenyl]benzonitrile

Suppliers and Price of 4-(6-Hydroxyhexyloxy)-4'-cyanoazobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 0 raw suppliers

Chemical Property of 4-(6-Hydroxyhexyloxy)-4'-cyanoazobenzene

Chemical Property:

Boiling Point:528.4±40.0 °C(Predicted)
PSA：77.97000
Density:1.10±0.1 g/cm3(Predicted)
LogP:4.90518
XLogP3:4.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:9
Exact Mass:323.16337692
Heavy Atom Count:24
Complexity:402

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1C#N)N=NC2=CC=C(C=C2)OCCCCCCO

Technology Process of 4-(6-Hydroxyhexyloxy)-4'-cyanoazobenzene

There total 4 articles about 4-(6-Hydroxyhexyloxy)-4'-cyanoazobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 2009-83-8
6-chloro-1-hexanol

: 107016-88-6,26029-68-5
4-[4-(cyanophenyl)azo]phenol

: 88216-53-9
4-[4-(6-hydroxyhexyloxy)phenylazo]benzonitrile

Guidance literature:: With potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; at 110 ℃; for 12h;
DOI:10.1039/c4ra09863c

Reference yield:

: 873-74-5
4-Aminobenzonitrile

: 88216-53-9
4-[4-(6-hydroxyhexyloxy)phenylazo]benzonitrile

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride; sodium nitrite / water / 0.17 h / 0 °C

1.2: 2 h / 0 °C

2.1: potassium iodide; potassium carbonate / N,N-dimethyl-formamide / 12 h / 110 °C

With hydrogenchloride; potassium carbonate; potassium iodide; sodium nitrite; In water; N,N-dimethyl-formamide;
DOI:10.1039/c4ra09863c

Reference yield:

: 108-95-2,27073-41-2
phenol

: 88216-53-9
4-[4-(6-hydroxyhexyloxy)phenylazo]benzonitrile

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride; sodium nitrite / water / 0.17 h / 0 °C

1.2: 2 h / 0 °C

2.1: potassium iodide; potassium carbonate / N,N-dimethyl-formamide / 12 h / 110 °C

With hydrogenchloride; potassium carbonate; potassium iodide; sodium nitrite; In water; N,N-dimethyl-formamide;
DOI:10.1039/c4ra09863c