9H-Fluorene, 9-butyl-9-(phenylmethyl)-

Base Information

Chemical Name:9H-Fluorene, 9-butyl-9-(phenylmethyl)-
CAS No.:88223-32-9
Molecular Formula:C24H24
Molecular Weight:312.455
Hs Code.:

Synonyms:

Suppliers and Price of 9H-Fluorene, 9-butyl-9-(phenylmethyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 9H-Fluorene, 9-butyl-9-(phenylmethyl)-

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 9H-Fluorene, 9-butyl-9-(phenylmethyl)-

There total 5 articles about 9H-Fluorene, 9-butyl-9-(phenylmethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 109-65-9
1-bromo-butane

: 1572-46-9
9-benzylfluorene

: 88223-32-9
9-benzyl-9-butyl-fluorene

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydroxide; In water; at 80 ℃; for 24h; Inert atmosphere; Sealed tube;
DOI:10.1039/c6gc02518h

Reference yield:

: 86-73-7
9H-fluorene

: 88223-32-9
9-benzyl-9-butyl-fluorene

Guidance literature:: Multi-step reaction with 2 steps

1: cesiumhydroxide monohydrate / toluene / 12 h / 130 °C / Sealed tube; Inert atmosphere; Green chemistry

2: tetra-(n-butyl)ammonium iodide; sodium hydroxide / water / 24 h / 80 °C / Inert atmosphere; Sealed tube

With cesiumhydroxide monohydrate; tetra-(n-butyl)ammonium iodide; sodium hydroxide; In water; toluene;
DOI:10.1039/c6gc02518h

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 88223-32-9
9-benzyl-9-butyl-fluorene

Guidance literature:: Multi-step reaction with 2 steps

1: cesiumhydroxide monohydrate / toluene / 12 h / 130 °C / Sealed tube; Inert atmosphere; Green chemistry

2: tetra-(n-butyl)ammonium iodide; sodium hydroxide / water / 24 h / 80 °C / Inert atmosphere; Sealed tube

With cesiumhydroxide monohydrate; tetra-(n-butyl)ammonium iodide; sodium hydroxide; In water; toluene;
DOI:10.1039/c6gc02518h