(Prop-2-en-1-yl)tris(2,4,6-trimethylphenyl)stannane

Base Information

Chemical Name:(Prop-2-en-1-yl)tris(2,4,6-trimethylphenyl)stannane
CAS No.:88259-29-4
Molecular Formula:C30H38Sn
Molecular Weight:517.342
Hs Code.:
DSSTox Substance ID:DTXSID80521405

Synonyms:88259-29-4;(Prop-2-en-1-yl)tris(2,4,6-trimethylphenyl)stannane;DTXSID80521405

Suppliers and Price of (Prop-2-en-1-yl)tris(2,4,6-trimethylphenyl)stannane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of (Prop-2-en-1-yl)tris(2,4,6-trimethylphenyl)stannane

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:5
Exact Mass:518.199554
Heavy Atom Count:31
Complexity:485

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C(C(=C1)C)[Sn](CC=C)(C2=C(C=C(C=C2C)C)C)C3=C(C=C(C=C3C)C)C)C

Technology Process of (Prop-2-en-1-yl)tris(2,4,6-trimethylphenyl)stannane

There total 1 articles about (Prop-2-en-1-yl)tris(2,4,6-trimethylphenyl)stannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 6166-12-7
tris(2,4,6-trimethylphenyl)tin(IV) bromide

: 1730-25-2
allylmagnesium bromide

: 88259-29-4
allyltris(2,4,6-trimethylphenyl)stannane

Guidance literature:: In diethyl ether; toluene; byproducts: MgBr2; toluene soln. of stannane added to organomagnesium compd. (prepd. in dry ether); heated at the b.p. of toluene (ether distd. off) until a test for bromine was neg. (15 h); cooled; hydrolyzed; org. layer sepd., washed, dried, solvent driven off; recrystd. (propyl alcohol); IR; PMR; elem. anal.;

Reference yield:

: 88259-29-4
allyltris(2,4,6-trimethylphenyl)stannane

: trityl tetrakis(pentafluorophenyl)borate

: trimesitylstannylium tetrakis(pentafluorophenyl)borate

Guidance literature:: With triethylsilane; In benzene-d6; byproducts: triphenylmethane; N2-atmosphere, glovebox; Et3SiH addn., top phase removing, diphenylethene addn., stannane soln. addn., top phase removing; not isolated, detd by NMR spectroscopy;
DOI:10.1021/ja990389u