Germane, 1,4-phenylenebis(trimethyl-)-

Base Information

Chemical Name:Germane, 1,4-phenylenebis(trimethyl-)-
CAS No.:21364-16-9
Molecular Formula:C12H22Ge2
Molecular Weight:311.487
Hs Code.:
DSSTox Substance ID:DTXSID40175625
Wikidata:Q83045969

Synonyms:21364-16-9;Germane, 1,4-phenylenebis(trimethyl-)-;Germane, 1,4-phenylenebis[trimethyl-]-;1,4-bis(trimethylgermyl)benzene;DTXSID40175625;InChI=1/C12H22Ge2/c1-13(2,3)11-7-9-12(10-8-11)14(4,5)6/h7-10H,1-6H

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Germane, 1,4-phenylenebis(trimethyl-)-

Chemical Property:

Vapor Pressure:0.0139mmHg at 25°C
Boiling Point:266.8°C at 760 mmHg
Flash Point:110°C
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:2
Exact Mass:312.0154043
Heavy Atom Count:14
Complexity:156

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[Ge](C)(C)C1=CC=C(C=C1)[Ge](C)(C)C

Technology Process of Germane, 1,4-phenylenebis(trimethyl-)-

There total 3 articles about Germane, 1,4-phenylenebis(trimethyl-)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 624-38-4,1032416-46-8
para-diiodobenzene

: 917-54-4
methyllithium

: 22702-77-8
1,2-dichlorotetramethyldigermane

: 21364-16-9
p-bis(trimethylgermyl)benzene

Guidance literature:: tetrakis(triphenylphosphine) palladium⁽⁰⁾; In benzene; 120°C for 10 h;

Reference yield: 42.0%

: 1529-47-1
chlorotrimethylgermane

: 21364-16-9
p-bis(trimethylgermyl)benzene

Guidance literature:: With magnesium; 1,4-dihalogenobenzene; In tetrahydrofuran; the aromatic halogeno-compd. was added to the soln. of Mg and trimethylchloro-compd., refluxed for several d; hydrolysed with dild. HCl, extd. with ether, dried over Na2SO4, the solvent evapd., the product recrystd. from methanol; elem. anal.;